1,4-二甲基-2-吡咯烷酮合成路线 （共 9 条）
反应条件
hydrogen; 5 rhodium-on-charcoal in water
T=20 - 200°C; P=75007.5 - 187519 Torr; 67 h; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2011/251119 A1, 2011 ;
Location in patent: Page/Page column 11 ;
反应条件
hydrogen; 5 rhodium-on-charcoal in water
T=20 - 200°C; P=75007.5 - 150015 Torr; 65 h; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2011/251119 A1, 2011 ;
Location in patent: Page/Page column 12 ;
反应条件
hydrogen; 5 wt. ruthenium on carbon in water
T=20 - 200°C; P=37503.8 - 150015 Torr; 24 h; Autoclave; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2011/251119 A1, 2011 ;
Location in patent: Page/Page column 12 ;
反应条件
hydrogen; 5 rhodium-on-charcoal in water
T=20°C; P=37503.8 - 150015 Torr; 24 h; Autoclave; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2011/251119 A1, 2011 ;
Location in patent: Page/Page column 13 ;
反应条件
hydrogen; 5 wt. ruthenium on carbon in water
T=20 - 200°C; P=37503.8 - 150015 Torr; 24 h; Autoclave; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2011/251119 A1, 2011 ;
Location in patent: Page/Page column 13 ;
反应条件
hydrogen; 5 wt. ruthenium on carbon in water
T=20 - 200°C; P=37503.8 - 150015 Torr; 24 h; Autoclave; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2011/251119 A1, 2011 ;
Location in patent: Page/Page column 12 ;
反应条件
hydrogen; 5 rhodium-on-charcoal in water
T=20 - 200°C; P=37503.8 - 187519 Torr; 72 h; Autoclave; Product distribution / selectivity;
参考文献
BASF SE
Patent: US2011/251119 A1, 2011 ;
Location in patent: Page/Page column 11-12 ;
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene
T=80°C; 1 h;
参考文献
Sato, Tatsunori; Wada, Yasuko; Nishimoto, Mami; Ishibashi, Hiroyuki; Ikeda, Masazumi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 879 - 886
反应条件
1: 29 percent / Bu3SnH, AIBN / benzene / 3 h / 80 °C
2: 24 percent / Bu3SnH, AIBN / benzene / 1 h / 80 °C
View Scheme
参考文献
Sato, Tatsunori; Wada, Yasuko; Nishimoto, Mami; Ishibashi, Hiroyuki; Ikeda, Masazumi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 879 - 886
