3,3-二甲基丙烯酸三甲基硅酯合成路线 （共 13 条）
反应条件
pyridine in diethyl ether 3 h; Heating;
参考文献
Bellassoued, M.; Habbachi, F.; Gaudemar, M.
Synthesis, 1983 , # 9 p. 745 - 746
反应条件
triethylamine in dichloromethane 0.5 h; Ambient temperature;
参考文献
Synthesis, , # 8 p. 684 - 686
参考文献
Khan; Blessing; Schmidt
Synthesis, 1994 , # 3 p. 255 - 257
反应条件
boron trifluoride diethyl etherate
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 48, # 6 p. 1363 - 1368,1249 - 1253
反应条件
dibromotriphenyl-phosphorane 0.25 h; Ambient temperature; Yield given;
参考文献
Aizpurua, Jesus Mari; Palomo, Claudio
Synthesis, 1982 , # 8 p. 684 - 686
反应条件
1: BuLi/i-Pr2NH / tetrahydrofuran / - 20 deg C, 30 min, then rt., 12 h 2: 2.) 5percent HCl / 1.) toluene, 80-100 deg C, 12 h; 2.) MeOH, rt., 10 h View Scheme
参考文献
Khan; Blessing; Schmidt
Synthesis, 1994 , # 3 p. 255 - 257
反应条件
1: triphenylphosphine dibromide / 0.25 h / Ambient temperature 2: 2-oxo-3-trimethyltetrahydro-1,3-oxazole / 0.25 h / Ambient temperature View Scheme
参考文献
Aizpurua, Jesus Mari; Palomo, Claudio
Synthesis, 1982 , # 8 p. 684 - 686
反应条件
1: BuLi/i-Pr2NH / tetrahydrofuran / - 20 deg C, 30 min, then rt., 12 h 2: 2.) 5percent HCl / 1.) toluene, 80-100 deg C, 3 h; 2.) MeOH, rt., 10 h View Scheme
参考文献
Khan; Blessing; Schmidt
Synthesis, 1994 , # 3 p. 255 - 257
反应条件
1: BuLi/i-Pr2NH / tetrahydrofuran / - 20 deg C, 30 min, then rt., 12 h
2: 2.) 5percent HCl / 1.) toluene, 80-100 deg C, 12 h; 2.) MeOH, rt., 10 h
View Scheme
参考文献
Khan; Blessing; Schmidt
Synthesis, 1994 , # 3 p. 255 - 257
反应条件
lithium diisopropyl amide
2 h; Ambient temperature;
参考文献
Brady, William T.; Agho, Michael O.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 501 - 506
