2,2,2-三氯乙酰亚胺酸甲酯合成路线 (共 28 条)
参考文献
Chemische Berichte, , vol. 91, p. 1562,1566
参考文献
Chemische Berichte, , vol. 40, p. 1644
Journal fuer Praktische Chemie (Leipzig), , vol. <2>81, p. 202
反应条件
1: 5-nitro-1H-indazole With trifluorormethanesulfonic acid in dichloromethane T=25 - 35°C; Inert atmosphere; 2: methyl 2,2,2-trichloroacetimidate in dichloromethane T=20°C; Inert atmosphere; regioselective reaction;
参考文献
Baddam, Sudhakar Reddy; Uday Kumar; Panasa Reddy; Bandichhor, Rakeshwar
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1661 - 1663
参考文献
Cramer; Gaertner
Chemische Berichte, 1958 , vol. 91, p. 1562,1566
反应条件
1: 7-nitro-1H-indazole With trifluorormethanesulfonic acid in dichloromethane T=25 - 35°C; Inert atmosphere; 2: methyl 2,2,2-trichloroacetimidate in dichloromethane T=20°C; Inert atmosphere; regioselective reaction;
参考文献
Tetrahedron Letters, , vol. 54, # 13 p. 1661 - 1663
参考文献
Societe L'Oreal S.A.
Patent: US6221343 B1, 2001 ;
参考文献
Sinha, Hermant K.; Dogra, Sneh K.
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 8 p. 2668 - 2675
反应条件
1: 4-nitro-1H-indazole With trifluorormethanesulfonic acid in dichloromethane T=25 - 35°C; Inert atmosphere; 2: methyl 2,2,2-trichloroacetimidate in dichloromethane T=20°C; Inert atmosphere; regioselective reaction;
参考文献
Baddam, Sudhakar Reddy; Uday Kumar; Panasa Reddy; Bandichhor, Rakeshwar
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1661 - 1663
反应条件
1: C8H7IN2 With trifluorormethanesulfonic acid in dichloromethane T=25 - 35°C; Inert atmosphere; 2: methyl 2,2,2-trichloroacetimidate in dichloromethane T=20°C; Inert atmosphere; regioselective reaction;
参考文献
Baddam, Sudhakar Reddy; Uday Kumar; Panasa Reddy; Bandichhor, Rakeshwar
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1661 - 1663
参考文献
Cramer; Gaertner
Chemische Berichte, 1958 , vol. 91, p. 1562,1566