2,2,2-三氯乙酰亚胺酸甲酯合成路线 （共 28 条）
反应条件
in diethyl ether 3 h; Heating;
参考文献
Liebigs Annalen der Chemie, , # 1 p. 70 - 84
反应条件
in methanol; diethyl ether 1 h; Ambient temperature;
参考文献
Schwoebel, Alfred; Lux, Rudolf; Kresze, Guenter
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 35, p. 1 - 4
反应条件
Manganese (II) acetate in methanol T=20°C; 48 h; different trichloroacetonitrile concentration, other products;
参考文献
Suematsu, Kazumi
Chemical & Pharmaceutical Bulletin, 1984 , vol. 32, p. 291 - 294
参考文献
Chemische Berichte, , vol. 40, p. 1644
Journal fuer Praktische Chemie (Leipzig), , vol. <2>81, p. 202
反应条件
acetic acid T=20°C; 1.16667 h; Cooling;
参考文献
Zhang, Lei; Chen, Xiaojie; Liu, Jun; Zhu, Qingzhang; Leng, Ying; Luo, Xiaomin; Jiang, Hualiang; Liu, Hong
European Journal of Medicinal Chemistry, 2012 , vol. 58, p. 624 - 639
反应条件
1: 3-methyl-6-nitro-1H-indazole With trifluorormethanesulfonic acid in dichloromethane T=25 - 35°C; Inert atmosphere; 2: methyl 2,2,2-trichloroacetimidate in dichloromethane T=20°C; Inert atmosphere; regioselective reaction;
参考文献
Tetrahedron Letters, , vol. 54, # 13 p. 1661 - 1663
反应条件
in methanol Heating;
参考文献
Holan,G. et al.
Journal of the Chemical Society [Section] C: Organic, 1967 , p. 20 - 25
参考文献
Schaefer,F.C.; Peters,G.A.
Journal of Organic Chemistry, 1961 , vol. 26, p. 2778 - 2784
参考文献
Chemische Berichte, , vol. 91, p. 1562,1566
反应条件
1: 6-nitro-1H-indazole With trifluorormethanesulfonic acid in dichloromethane T=25 - 35°C; Inert atmosphere; 2: methyl 2,2,2-trichloroacetimidate in dichloromethane T=20°C; Inert atmosphere; regioselective reaction;
参考文献
Baddam, Sudhakar Reddy; Uday Kumar; Panasa Reddy; Bandichhor, Rakeshwar
Tetrahedron Letters, 2013 , vol. 54, # 13 p. 1661 - 1663
