3-(异丁烯酰氧)丙基三甲氧基硅烷合成路线 （共 21 条）
反应条件
triethylamine in methanol; toluene T=25°C; 6 h; Industry scale;
参考文献
ASAHI KASEI CHEMICALS CORPORATION
Patent: US2010/81837 A1, 2010 ;
Location in patent: Page/Page column 14 ;
参考文献
G-C Dental Industrial Corporation
Patent: US4713403 A1, 1987 ;
反应条件
pyridine in methanol; hexane; water T=2 - 20°C; 3 h;
参考文献
US2014/128564 A1, ;
Paragraph 0275 ;
反应条件
in methanol; hexane; water
反应条件
in methanol; hexane; water T=20°C; 3 h; Product distribution / selectivity;
参考文献
WO2008/42158 A1, ;
Page/Page column 39 ;
参考文献
G-C Dental Industrial Corporation
Patent: US4713403 A1, 1987 ;
反应条件
1: bis-trimethylsilyl ether With methanol; sulfuric acid T=5 - 10°C; 1 h; 2: methacrylic acid-3-trimethoxysilylpropyl ester T=5 - 10°C; 1.5 h; 3: With sulfuric acid; water more than 3 stages;
参考文献
EP1510520 A1, ;
Page/Page column 13 ;
反应条件
1: With sulfuric acid; acetic acid; trifluorormethanesulfonic acid T=-15 - 20°C; 2: With 1,1,1,3,3,3-hexamethyl-disilazane T=20°C; 2 h; Product distribution / selectivity;
参考文献
US2010/29972 A1, ;
Page/Page column 4 ;
反应条件
in methanol; hexane; water T=20°C; 3 h; Product distribution / selectivity;
参考文献
WO2008/42158 A1, ;
Page/Page column 40 ;
反应条件
in methanol; hexane; water
T=20°C; 3 h; Product distribution / selectivity;
参考文献
JOHNSON and JOHNSON VISION CARE, INC.; TORAY INDUSTRIES, INC.
Patent: WO2008/42158 A1, 2008 ;
Location in patent: Page/Page column 39 ;
