2-甲基-1,2-苯并噻唑-3-酮合成路线 （共 65 条）
反应条件
sodium tetrahydroborate
参考文献
Pinna, Giovanni; Bellucci, Maria Cristina; Malpezzi, Luciana; Pisani, Laura; Superchi, Stefano; Volonterio, Alessandro; Zanda, Matteo
Tetrahedron, 2011 , vol. 67, # 29 p. 5268 - 5281
参考文献
McClelland; Warren; Jackson
Journal of the Chemical Society, 1929 , p. 1585
参考文献
McClelland; Gait
Journal of the Chemical Society, 1926 , p. 923
反应条件
copper(l) iodide; 1,10-phenanthroline; potassium carbonate; sulfur in N,N-dimethyl-formamide
T=110°C; 3 h; Inert atmosphere;
参考文献
Bhakuni, Bhagat Singh; Balkrishna, Shah Jaimin; Kumar, Amit; Kumar, Sangit
Tetrahedron Letters, 2012 , vol. 53, # 11 p. 1354 - 1357
反应条件
2,4,6-trimethyl-pyridine; oxalyl dichloride in dichloromethane
T=-50°C; non-oxidative chloro-Pummerer reaction; Inert atmosphere;
参考文献
Pinna, Giovanni; Bellucci, Maria Cristina; Malpezzi, Luciana; Pisani, Laura; Superchi, Stefano; Volonterio, Alessandro; Zanda, Matteo
Tetrahedron, 2011 , vol. 67, # 29 p. 5268 - 5281
反应条件
2,4,6-trimethyl-pyridine; trifluoromethylsulfonic anhydride in acetonitrile
T=0°C; non-oxidative Pummerer reaction; Inert atmosphere;
参考文献
Pinna, Giovanni; Bellucci, Maria Cristina; Malpezzi, Luciana; Pisani, Laura; Superchi, Stefano; Volonterio, Alessandro; Zanda, Matteo
Tetrahedron, 2011 , vol. 67, # 29 p. 5268 - 5281
反应条件
potassium carbonate in acetonitrile
T=20°C; 2 h;
参考文献
ROHM AND HAAS COMPANY; DOW GLOBAL TECHNOLOGIES LLC; STEPHENS, Randall W.; EMONDS, Mark V. M.; HENTON, Daniel R.
Patent: WO2014/85138 A1, 2014 ;
Location in patent: Page/Page column 5 ;
反应条件
sodium hydroxide in dimethyl sulfate
参考文献
Kajiwara, Masahiro
Patent: US2003/60482 A1, 2003 ;
反应条件
potassium carbonate in tetrahydrofuran
T=20 - 25°C; 2 h;
参考文献
Liu, Dazhi; Tian, Zhen; Yan, Zhihui; Wu, Lixin; Ma, Yan; Wang, Quan; Liu, Wei; Zhou, Honggang; Yang, Cheng
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 11 p. 2960 - 2967
反应条件
trifluoroacetic acid; bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane
T=0°C; 1 h;
参考文献
Correa, Arkaitz; Tellitu, Imanol; Dominguez, Esther; SanMartin, Raul
Organic Letters, 2006 , vol. 8, # 21 p. 4811 - 4813
