O,O-二乙基硫代磷酰氯合成路线 (共 132 条)
参考文献
Journal of the American Chemical Society, , vol. 67, p. 1663
Journal of the American Chemical Society, , vol. 75, p. 6357
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 13, p. 269 - 278
反应条件
trichlorophosphate T=20°C; multistep reaction; varying of molar ratio of components; time taken in the addition of alcohol; consumption time of reactants; alcoholysis of PSCl3 (estimation of rel. rates); Product distribution;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 57, # 10 p. 2304 - 2310,2059 - 2065
反应条件
in dichloromethane 1) -20 deg C to RT, 2) RT, 10 min;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 851 - 854
参考文献
Sci.Rep.Res.Inst.Tohoku Univ.<A>, , vol. 4, p. 403,407
Gazzetta Chimica Italiana, , vol. 81, p. 596,604
Huaxue Xuebao, , vol. 22, p. 49,52,54
Chem.Abstr., , p. 6156
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 58, # 1-4 p. 61 - 88
反应条件
1: 3-chloro-4-methyl-7-hydroxycoumarin With n-butyllithium in tetrahydrofuran; hexane 1 h; 2: O,O-diethyl chlorothiophosphate in tetrahydrofuran; hexane T=20°C; 12 h;
参考文献
Journal of Medicinal Chemistry, , vol. 49, # 1 p. 246 - 255
反应条件
in N,N-dimethyl-formamide
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 40, # 4 p. 339 - 341