O,O-二乙基硫代磷酰氯合成路线 （共 132 条）
反应条件
(i) CH2Cl2, (ii) aq. NaI; Multistep reaction;
参考文献
Kolind-Andersen,H.; Lawesson,S.-O.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1975 , vol. 29, p. 430 - 440
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane
T=20°C; 0.5 h;
参考文献
Jones, R. Alan; Badesha, Santokh Singh
Synthetic Communications, 1981 , vol. 11, # 7 p. 557 - 560
反应条件
(i) CH2Cl2, (ii) aq. NaI; Multistep reaction;
参考文献
Kolind-Andersen,H.; Lawesson,S.-O.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1975 , vol. 29, p. 430 - 440
反应条件
potassium carbonate; acetone
参考文献
Losco; Peri
Gazzetta Chimica Italiana, 1959 , vol. 89, p. 1298,1304
反应条件
in chloroform
T=40 - 45°C;
参考文献
Tang, Chu Chi; Wu, Gui Ping; He, Shui Ji; He, Zheng Jie
Phosphorus, Sulfur and Silicon and the Related Elements, 1995 , vol. 101, # 1-4 p. 91 - 94
反应条件
pyridine; chlorobenzene
参考文献
Sen Gupta,A.K.; Kumar,J.
Journal of the Indian Chemical Society, 1966 , vol. 43, p. 575 - 577
反应条件
sodium carbonate; butanone
参考文献
Virginia Carolina Chem. Corp.
Patent: US2761806 , 1954 ;
参考文献
Michalski,J. et al.
Bulletin de l'Academie Polonaise des Sciences, Serie des Sciences Chimiques, 1965 , vol. 13, p. 677 - 682
反应条件
sodium carbonate; butanone
参考文献
Virginia Carolina Chem. Corp.
Patent: US2761806 , 1954 ;
反应条件
T=60°C; Rate constant;
参考文献
Lebedev, N. N.; Kiryushatova, T. V.; Savel'yanov, V. P.
J. Gen. Chem. USSR (Engl. Transl.), 1984 , vol. 54, # 9 p. 2141 - 2144,1913 - 1915
