1,2-bis-(diphenylphosphino)ethane; dihydridotetrakis(triphenylphosphine)ruthenium(II) in tetrahydrofuran T=60°C; overnight; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 111, # 15 p. 5954 - 5955
2,2'-azo-bisisobutyronitrile in neat (no solvent) mixt. of org. and Sn educts (1/0.5 ratio) and azobisisobutyronitrile under N2 at 80°C reacted for 2 h; chromd. (SiO2, CCl4), recrystd. (EtOH);
参考文献
Journal of Organometallic Chemistry, , vol. 212, # 2 p. 163 - 170
