aluminium trichloride T=100°C;

ammonium chloride; zinc in ethanol T=80°C; 0.00833333 h; microwave irradiation;

aluminium trichloride; chlorine

1: aqueous hydrochloric acid; sodium nitrite / Eintragen der erhaltenen Diazoniumsalz-Loesung in eine mit Benzol ueberschichtete wss. Alkali-tetracyanocuprat(I)-Loesung 2: diethyl ether / anschliessendes Behandeln mit wss. HCl View Scheme

diethyl ether anschliessendes Behandeln mit wss. HCl;

aluminium trichloride; chlorine

hydrogen bromide; dihydrogen peroxide in 1,4-dioxane; water 20 h; Heating;

copper(ll) bromide in chloroform; ethyl acetate 5 h; Reflux;

1.1: potassium carbonate / copper / 10 h / 130 °C 2.1: morpholine; sulfur / 12 h / 110 °C 2.2: 8 h / Reflux 3.1: sulfuric acid / 2 h / 50 °C 4.1: sodium t-butanolate / tert-butyl methyl ether / 2 h / 5 - 20 °C 5.1: (S)-pyrophosphoric acid / water / 2 h / 0 - 60 °C 6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / 20 - 35 °C 7.1: hydrogen / Ni-Raney / tetrahydrofuran / 48 h / 20 °C / 2585.81 - 3102.97 Torr 8.1: ethyl acetate / 96 h / 25 °C 9.1: boron trifluoride diethyl etherate; triethylsilane / 24 h / 105 °C 10.1: sodium hydroxide / dichloromethane; water / pH > 10 10.2: 2 h / 60 °C View Scheme

iodine 4 h; Heating;