1,7-二氯辛甲基四硅氧烷合成路线 （共 12 条）
反应条件
CuI; triphenylphosphine; (PPh3)2PdCl2 in triethylamine; toluene
反应条件
water in 1,4-dioxane; diethyl ether; water addn. of H2O (8.3 mol) in dioxane to a soln. of (CH3)2SiCl2 (16.6 mol) in ether;;
参考文献
US2381366 , ;
C. A., , p. 4890
反应条件
1,4-dioxane; diethyl ether; water
参考文献
Journal of the American Chemical Society, , vol. 68, p. 360,363
US2381366 , ;
反应条件
dimethyl sulfoxide T=0 - 20°C; 3 h; Reagent/catalystSolvent;
参考文献
Doklady Chemistry, , vol. 451, # 2 p. 203 - 206
Dokl. Akad. Nauk, , vol. 451, # 5 p. 528 - 532
反应条件
water; carbon 4 h; Ambient temperature;
参考文献
Chemistry Letters, , # 11 p. 2133 - 2136
反应条件
aluminium trichloride in neat (no solvent) ((CH3)2SiO)4 and AlCl3 at about 120°C;;
参考文献
US2645654 , ;
C. A., , p. 7050
反应条件
sodium nitrate T=0°C; 2 h; Yield givenFurther byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Russian Journal of General Chemistry, , vol. 68, # 4 p. 658 - 659
Zhurnal Obshchei Khimii, , vol. 68, # 4 p. 699 - 700
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 806,807, 809; engl. Ausg. S. 827, 828, 830
反应条件
CoCl2 in acetonitrile 168 h; Ambient temperatureother acyl chlorides; also in the presence of hexamethyldisiloxane or trimethylacetoxysilane; Product distribution;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 62, # 1.1 p. 97 - 102,79 - 83
反应条件
tetrahydrofuran; lt;Mg2Cl3(THF)4gt;+lt;AlH3Clgt;- 2 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Knott, Wilfried
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 1997 , vol. 52, # 5 p. 629 - 634
