N-苄氧羰基-D-苯丙氨酸合成路线 (共 60 条)
参考文献
Pearson; Shin
Journal of Organic Chemistry, 1994 , vol. 59, # 9 p. 2314 - 2323
反应条件
S-1-methylheptanol; borate buffer; water; Bis-(S)-2-octyl sodium sulphosuccinate; 1H-imidazole in n-heptane T=25°C; kD; pH= 8.0; other catalyst, other racemic or chiral surfactant and cosurfactants and other proportions of water and surfactant; Rate constant;
参考文献
Tetrahedron, , vol. 43, # 1 p. 77 - 84
反应条件
trifluoroacetic acid T=20°C; 0.5 h;
参考文献
Harding, Christopher I.; Dixon, Darren J.; Ley, Steven V.
Tetrahedron, 2004 , vol. 60, # 35 p. 7679 - 7692
反应条件
10 Pd/C; cyclohexa-1,4-diene in ethyl acetate T=100°C; 0.0833333 h; Microwave irradiation;
参考文献
Quinn, John F.; Razzano, Dana A.; Golden, Kathryn C.; Gregg, Brian T.
Tetrahedron Letters, 2008 , vol. 49, # 42 p. 6137 - 6140
反应条件
1: 69 percent / BF3*THF / CH2Cl2 / 2 h / 30 °C 2: 64 percent / KHMDS / tetrahydrofuran; toluene / -78 - 20 °C 3: 85 percent / aq. NaIO4; RuCl3; NaHCO3 / acetonitrile; CCl4 / 2 h / 20 °C 4: 74 percent / BuLi; diisopropylamine; HMPA / tetrahydrofuran; hexane / 21 h / -55 °C 5: 85 percent / aq. CF3CO2H / 0.5 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 35 p. 7679 - 7692
反应条件
1: 85 percent / aq. NaIO4; RuCl3; NaHCO3 / acetonitrile; CCl4 / 2 h / 20 °C 2: 74 percent / BuLi; diisopropylamine; HMPA / tetrahydrofuran; hexane / 21 h / -55 °C 3: 85 percent / aq. CF3CO2H / 0.5 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 35 p. 7679 - 7692
反应条件
1: 64 percent / KHMDS / tetrahydrofuran; toluene / -78 - 20 °C 2: 85 percent / aq. NaIO4; RuCl3; NaHCO3 / acetonitrile; CCl4 / 2 h / 20 °C 3: 74 percent / BuLi; diisopropylamine; HMPA / tetrahydrofuran; hexane / 21 h / -55 °C 4: 85 percent / aq. CF3CO2H / 0.5 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 35 p. 7679 - 7692
反应条件
citrate buffer; dl-cysteine hydrochloride; papain T=50°C; 24 h;
参考文献
Synthetic Communications, , vol. 18, # 4 p. 441 - 444
反应条件
phosphate buffer; α-chymotrypsin in dimethyl sulfoxide T=-24°C; pH=8.0; 72 h;
参考文献
Salam, Sayed Mohiuddin Abdus; Kagawa, Ken-Ichi; Kawashiro, Katsuhiro
Tetrahedron Asymmetry, 2006 , vol. 17, # 1 p. 22 - 29
反应条件
sodium hydroxide; sodium hydrogencarbonate in 1,4-dioxane; water T=0°C;
参考文献
Organic Letters, , vol. 8, # 2 p. 239 - 242