2,6-二叔丁基对苯二酚合成路线 （共 46 条）
反应条件
2,6-di-tert-butyl-4-methyl-phenol in benzene
T=19.85°C; Equilibrium constantThermodynamic data; Further Variations:Solvents;
参考文献
Lucarini, Marco; Mugnaini, Veronica; Pedulli, Gian Franco; Guerra, Maurizio
Journal of the American Chemical Society, 2003 , vol. 125, # 27 p. 8318 - 8329
反应条件
1: 11 percent Spectr. / PhOH, pyridine / nitromethane / 8 h / Ambient temperature
2: 1.95 g / NaBH4 / methanol / 0.08 h
View Scheme
参考文献
Karhu, Matti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 303 - 306
反应条件
tert-butyl alcohol
T=27°C; 0.0333333 h; Further byproducts given. Yields of byproduct given;
参考文献
Omura, Kanji
Journal of Organic Chemistry, 1996 , vol. 61, # 20 p. 7156 - 7161
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Rieker,A. et al.
Z. Naturforsch., B: Anorg. Chem., Org. Chem., Biochem., Biophys.,, 1964 , vol. 19, p. 558 - 560
反应条件
tert.-butyl lithium in diethyl ether; pentane
参考文献
Nishinaga,A. et al.
Chemische Berichte, 1976 , vol. 109, p. 1530 - 1548
反应条件
silver perchlorate; sodium carbonate
T=0°C; 0.0333333 h; Yield given. Yields of byproduct given;
参考文献
Omura, Kanji
Journal of Organic Chemistry, 1996 , vol. 61, # 20 p. 7156 - 7161
反应条件
silver perchlorate; sodium carbonate
T=0°C; 0.0333333 h; Yield given. Yields of byproduct given;
参考文献
Omura, Kanji
Journal of Organic Chemistry, 1996 , vol. 61, # 20 p. 7156 - 7161
反应条件
silver perchlorate; sodium carbonate
T=0°C; 0.0333333 h; Yield given. Yields of byproduct given;
参考文献
Omura, Kanji
Journal of Organic Chemistry, 1996 , vol. 61, # 20 p. 7156 - 7161
反应条件
1: PhOH, conc. H2SO4 / 1,2-dimethoxy-ethane / 0.5 h / Ambient temperature
2: 1.95 g / NaBH4 / methanol / 0.08 h
View Scheme
参考文献
Karhu, Matti
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 303 - 306
反应条件
1: (i) O2, aq. KOH, EtOH, (ii) Me2S
2: tBuLi / pentane; diethyl ether
View Scheme
参考文献
Nishinaga,A. et al.
Chemische Berichte, 1976 , vol. 109, p. 1530 - 1548
