反式-9,10-环氧十八烷酸合成路线 （共 8 条）
反应条件
1: sulfuric acid / acetonitrile; water / 16 h / 20 °C 2: sodium periodate; sodium hydrogencarbonate / acetonitrile; water / 1.5 h / 20 °C View Scheme
参考文献
Spannring, Peter; Yazerski, Vital; Bruijnincx, Pieter C. A.; Weckhuysen, Bert M.; Klein Gebbink, Robertus J. M.
Chemistry - A European Journal, 2013 , vol. 19, # 44 p. 15012 - 15018
反应条件
H3[PW12O40]; dihydrogen peroxide; 1-hexadecylpyridinium bromide in water T=85°C; 5 h; Green chemistry;
参考文献
JAOCS, Journal of the American Oil Chemists' Society, , vol. 90, # 1 p. 133 - 140
反应条件
hydrogenchloride; diethyl ether
参考文献
Kuranova,I.L.; Balykina,L.V.
Journal of Organic Chemistry USSR (English Translation), 1975 , vol. 11, p. 716 - 721
Zhurnal Organicheskoi Khimii, 1975 , vol. 11, p. 720 - 726
反应条件
H3[PW12O40]; dihydrogen peroxide; 1-hexadecylpyridinium bromide in water T=85°C; 5 h; Green chemistry;
参考文献
JAOCS, Journal of the American Oil Chemists' Society, , vol. 90, # 1 p. 133 - 140
反应条件
phosphorus pentoxide
参考文献
Nicolet; Poulter
Journal of the American Chemical Society, 1930 , vol. 52, p. 1189
反应条件
1: sulfuric acid / acetonitrile; water / 16 h / 20 °C
2: sodium periodate; sodium hydrogencarbonate / acetonitrile; water / 1.5 h / 20 °C
View Scheme
参考文献
Spannring, Peter; Yazerski, Vital; Bruijnincx, Pieter C. A.; Weckhuysen, Bert M.; Klein Gebbink, Robertus J. M.
Chemistry - A European Journal, 2013 , vol. 19, # 44 p. 15012 - 15018
反应条件
methylmagnesium N-cyclohexylisopropylamide in toluene
T=24°C; 20 h; added at 0 deg C;
参考文献
Mosset, Paul; Manna, Sukumar; Viala, Jacques; Falck, J.R.
Tetrahedron Letters, 1986 , vol. 27, # 3 p. 299 - 302
反应条件
in toluene
T=24°C; 20 h; added at 0 deg C;
参考文献
Mosset, Paul; Manna, Sukumar; Viala, Jacques; Falck, J.R.
Tetrahedron Letters, 1986 , vol. 27, # 3 p. 299 - 302
