1: With lithium in diethyl ether
4 h; RefluxInert atmosphere;
2: With mercury dichloride in diethyl ether
T=20°C; Inert atmosphere;
3: With selenium
T=200°C; Neat (no solvent)Inert atmosphere;
参考文献
Klapoetke, Thomas M.; Krumm, Burkhard; Scherr, Matthias
Zeitschrift fur Anorganische und Allgemeine Chemie, 2010 , vol. 636, # 11 p. 1955 - 1961