2-[(2-甲基-2-丙基)二硫基]吡啶合成路线 （共 49 条）
反应条件
in chlorobenzene
T=133°C; 1 h; reaction with other alkene; Product distribution;
参考文献
Barton, Derek H. R.; Crich, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1613 - 1620
反应条件
in benzene
Irradiation;
参考文献
Newcomb, Martin; Esker, John L.
Tetrahedron Letters, 1991 , vol. 32, # 8 p. 1035 - 1038
反应条件
1: CH2Cl2 / 2 h / Heating
2: benzene / 2 h / 80 °C / Irradiation
View Scheme
参考文献
Beckwith, Athelstan L. J.; Duggan, Sandhya A. M.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1994 , # 7 p. 1509 - 1518
反应条件
4-(N,N-dimethlyamino)pyridine; dimethylsulfide; propionyl-1-14C chloride; oxygen
1) toluene, 80 deg C, 10 min, 2) toluene; Yield given. Multistep reaction;
参考文献
Barton, Derek H. R.; Crich, David; Motherwell, William B.
Journal of the Chemical Society, Chemical Communications, 1984 , # 4 p. 242 - 244
反应条件
oxygen; 2-methylpropane-2-thiol
1) toluene, irradiation, room temperature; 2) 0.1 M H3PO4/EtOH; Yield given. Multistep reaction;
参考文献
Barton, Derek H. R.; Crich, David; Motherwell, William B.
Tetrahedron, 1985 , vol. 41, # 19 p. 3901 - 3924
反应条件
oxalyl dichloride
1.) benzene, 18 h, 2.) chlorobenzene, reflux, 1 h; Yield given. Multistep reaction;
参考文献
Barton, Derek H. R.; Crich, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1603 - 1612
反应条件
in benzene
T=80°C; 3 h; Mechanism;
参考文献
Barton, Derek H. R.; Crich, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 1613 - 1620
反应条件
Yield given. Multistep reaction;
参考文献
Barton, Derek H. R.; Crich, David; Motherwell, William B.
Tetrahedron, 1985 , vol. 41, # 19 p. 3901 - 3924
反应条件
dimethylsulfide; oxygen; 2-methylpropane-2-thiol; 4-(N,N-dimethlyamino)pyridine
multistep reaction: 1) 80 deg C; 2) 80 deg C; investigation of reaction with various molar ratios and (MeO3)P; Product distribution;
参考文献
Barton, Derek H. R.; Crich, David; Motherwell, William B.
Tetrahedron, 1985 , vol. 41, # 19 p. 3901 - 3924
