N,N-二乙基-2,2,2-三氯-乙酰胺合成路线 （共 9 条）
参考文献
The United States of America as represented by the Secretary of the Navy
Patent: US6686494 B1, 2004 ;
Location in patent: Page column 9 ;
反应条件
1: With 1,4-diaza-bicyclo[2.2.2]octane; sulfur monochloride T=-10°C; 2: With formic acid Further stages.;
参考文献
Konstantinova; Berezin; Rakitin
Russian Chemical Bulletin, 2007 , vol. 56, # 6 p. 1178 - 1183
反应条件
in hexane 1.) 20-25 deg C, 20 min, 2.) boiling;;
参考文献
Migaichuk, I. V.; Khaskin, I. G.
J. Appl. Chem. USSR (Engl. Transl.), 1982 , vol. 55, # 9 p. 2066 - 2070,1900 - 1903
反应条件
(i) 3-trifluoromethyl-benzoyl fluoride, (ii) /BRN= 1737093/, Et2O; Multistep reaction;
参考文献
Boehme,H.; Hilp,M.
Chemische Berichte, 1970 , vol. 103, p. 104 - 111
反应条件
1: N,N-diethyl-α,α,α-trichloroacetamide in tetrahydrofuran T=20°C; 0.25 h; 2: 4-chlorophenylmethanethiol T=20°C; 4 h; Heating / reflux;
参考文献
The United States of America as represented by the Secretary of the Navy
Patent: US6686494 B1, 2004 ;
Location in patent: Page column 9-10 ;
反应条件
in tetrahydrofuran 16 h; Heating;
参考文献
Wynne, James H.; Jensen, Samuel D.; Snow, Arthur W.
Journal of Organic Chemistry, 2003 , vol. 68, # 9 p. 3733 - 3735
反应条件
nitronium tetrafluoroborate
T=40°C; var. ratio of reactants; Product distribution;
参考文献
Andreev, S. A.; Lebedev, B. A.; Tselinskii, I. V.; Shokhor, I. N.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 7 p. 1159 - 1166
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 7 p. 1353 - 1360
反应条件
tributylphosphine in chloroform
参考文献
Speziale,A.J.; Freeman,R.C.
Journal of the American Chemical Society, 1960 , vol. 82, p. 903 - 909
反应条件
phosphorous acid diethyl ester; triethylamine in benzene
12 h; Ambient temperature;
参考文献
Gertsyuk, M. N.; Dorokhov, V. I.; Samarai, L. I.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, # 4 p. 822 - 823
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 4 p. 903 - 904
