2-氯-5,5-二甲基-1,3,2-二氧磷杂环己烷合成路线 （共 28 条）
反应条件
phosphorus trichoride 1 h;
参考文献
Matos, Robson M.; Gomes De Lima, Luiz Carlos; De Souza, Edward; Barcelos De Souza, Ana Lucia Americano; Gomes De Lima, Miriam Bernardes; Soares Raslan, Delio
Phosphorus, Sulfur and Silicon and the Related Elements, 2002 , vol. 177, # 12 p. 2859 - 2870
反应条件
anhydrous phosphorus trichloride in toluene
参考文献
EASTMAN KODAK COMPANY
Patent: EP382660 A1, 1990 ;
反应条件
tetrachlorosilane; triethylamine in benzene 2 h; Ambient temperature;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 90, # 1-4 p. 243 - 248
反应条件
in benzene T=60°C; 1 h; Product distribution;
参考文献
Russian Journal of General Chemistry, , vol. 70, # 10 p. 1649 - 1650
Zhurnal Obshchei Khimii, , vol. 70, # 10 p. 1752 - 1753
反应条件
trimethylsilyl bromide in dichloromethane T=20°C; 2 h; Inert atmosphere;
参考文献
Dabkowski, Wojciech; Ozarek, Alfred; Olejniczak, Sebastian; Cypryk, Marek; Chojnowski, Julian; Michalski, Jan
Chemistry - A European Journal, 2009 , vol. 15, # 7 p. 1747 - 1756
反应条件
triethylamine 5 h; Heating;
参考文献
Nifantyev; Gratchev; Burmistrov Yu.; Vasyanina
Tetrahedron, 1991 , vol. 47, # 47 p. 9839 - 9860
反应条件
water T=20°C; Hydrolysis; 12 h;
参考文献
Muthiah; Praveen Kumar; Aruna Mani; Kumara Swamy
Journal of Organic Chemistry, 2000 , vol. 65, # 12 p. 3733 - 3737
反应条件
pyridine in diethyl ether
参考文献
Patois, Carl; Ricard, Louis; Savignac, Philippe
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 6 p. 1577 - 1581
反应条件
1: Et3N / benzene 2: tBuO2H 3: (i) NaH, (ii) CS2, (iii) /BRN= 969135/ View Scheme
参考文献
Journal of Organic Chemistry, , vol. 41, # 2 p. 227 - 233
反应条件
1: Py / diethyl ether 2: sulfur View Scheme
参考文献
Tetrahedron, , vol. 20, p. 2781 - 2795
