5,5-双(羟甲基)-2-苯基-1,3-二氧杂环己烷合成路线 (共 14 条)
反应条件
1: in pyridine
solid phase reaction; 16 h; Heating;
2: With potassium tert-butylate in tetrahydrofuran
T=20°C; 3 h;
参考文献
Behrendt, Jonathan M.; Bala, Kason; Golding, Peter; Hailes, Helen C.
Tetrahedron Letters, 2005 , vol. 46, # 4 p. 643 - 645
反应条件
pyridine
T=0°C; 20 h;
参考文献
Ashry, E. S. H. El; Kilany, Y. El; Hamid, H. Abdel; El-Zemity, S. R.; Boghdady, S.
Journal of Chemical Research, Miniprint, 2003 , # 1 p. 111 - 128
反应条件
toluene-4-sulfonic acid in toluene
Heating;
参考文献
Lemcoff, N Gabriel; Fuchs, Benzion
Organic letters, 2002 , vol. 4, # 5 p. 731 - 734
反应条件
pyridine; thionyl chloride; chloroform
参考文献
Wawzonek; Issidorides
Journal of the American Chemical Society, 1953 , vol. 75, p. 2373