in benzene (exclusion of moisture), ligand and Ti complex stirred in benzene at 30-40°C for 150 min; evapd.(vac.), dissolved (CS2), treated with n-pentane, cooled to -26°C, isolated, washed (n-pentane), dried (air), elem. anal.;
参考文献
European Journal of Inorganic Chemistry, , # 4 p. 718 - 725
in benzene (exclusion of moisture), ligand and Ti complex stirred in benzene at 30-40°C for 180 min; evapd.(vac.), dissolved (CS2), treated with n-pentane, cooled to -26°C for 15 h, isolated, washed (n-pentane), dried (air), elem. anal.;
参考文献
European Journal of Inorganic Chemistry, , # 4 p. 718 - 725
