1-(5-甲基-3-异噁唑)乙酮合成路线 （共 27 条）
参考文献
Palazzo et al.
Annali di Chimica (Rome, Italy), 1959 , vol. 49, p. 853,855
参考文献
Angelico; Calvello
Gazzetta Chimica Italiana, 1904 , vol. 34 I, p. 47
反应条件
in methanol Irradiation;
参考文献
Sauers, Ronald R.; Van Arnum, Susan D.
Tetrahedron Letters, 1987 , vol. 28, # 47 p. 5797 - 5800
参考文献
Sauers, Ronald R.; Van Arnum, Susan D.
Tetrahedron Letters, 1987 , vol. 28, # 47 p. 5797 - 5800
参考文献
Sauers, Ronald R.; Van Arnum, Susan D.
Tetrahedron Letters, 1987 , vol. 28, # 47 p. 5797 - 5800
反应条件
in acetonitrile Irradiationother solvent, sensitizer, additives; Product distribution;
参考文献
Sauers, Ronald R.; Van Arnum, Susan D.
Tetrahedron Letters, 1987 , vol. 28, # 47 p. 5797 - 5800
反应条件
in tetrahydrofuran T=0 - 20°C; 3.08333 h; Inert atmosphere;
参考文献
Genentech, Inc.
Patent: US2012/214762 A1, 2012 ;
Location in patent: Page/Page column 102 ;
反应条件
1: NaBH4 / methanol / 0.17 h / 20 °C 2: 1.74 g / pyridine / 12 h / 20 °C 3: 34 percent / tetrasulfur tetranitride antimony pentachloride complex / toluene / 1 h / 100 °C 4: 88 percent / NaOH / methanol / 0.5 h / 20 °C View Scheme
参考文献
Kim, Kil-Joong; Kim, Kyongtae
Tetrahedron, 2007 , vol. 63, # 23 p. 5014 - 5018
反应条件
hydrogenchloride; sulfuric acid; sodium nitrite in hydrogenchloride; ethanol; water
T=50°C; 6 h;
参考文献
Genentech, Inc.
Patent: US2012/214762 A1, 2012 ;
Location in patent: Page/Page column 102 ;
反应条件
sodium hydrogencarbonate in dichloromethane
Ambient temperature;
参考文献
Amici, Marco De; Micheli, Carlo De; Carrea, Giacomo; Spezia, Sandro
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2646 - 2650
