1-(二乙氧基甲基)-4-甲基苯合成路线 (共 16 条)
反应条件
zirconium tetrachloride 0.2 h;
参考文献
Karimi, Babak; Ashtiani, Ashraf Miri
Chemistry Letters, 1999 , # 11 p. 1199 - 1200
反应条件
ammonium chloride; orthoformic acid triethyl ester 0.75 h; Heating; Yield given;
参考文献
Maegawa, Tomohiro; Otake, Kazuki; Goto, Akihiro; Fujioka, Hiromichi
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 16 p. 5648 - 5651
反应条件
iodine; mercury(II) oxide in tetrachloromethane 5 h; Irradiation;
参考文献
Glover, Stephen A.; Golding, Stephen L.; Goosen, Andre; McCleland, Cedric W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2479 - 2483
反应条件
1: 90 percent / HClO4-SiO2 / H2O; methanol / 0.17 h / 25 - 30 °C 2: 95 percent / HClO4-SiO2 / 0.17 h / 25 - 30 °C View Scheme
参考文献
Kumar, Raj; Kumar, Dinesh; Chakraborti, Asit K.
Synthesis, 2007 , # 2 p. 299 - 303
反应条件
1: 1.) NaH / 2.) benzene, heating, 12 h 2: 50 percent / I2, HgO / CCl4 / 5 h / Irradiation View Scheme
参考文献
Glover, Stephen A.; Golding, Stephen L.; Goosen, Andre; McCleland, Cedric W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 10 p. 2479 - 2483
反应条件
piperidine; pyridine
参考文献
Klein; Bergmann
Journal of the American Chemical Society, 1957 , vol. 79, p. 3452
Full Text View citing articles Show Details
Jones; Watkinson
Journal of the Chemical Society, 1958 , p. 4064,4068
反应条件
1: piperidine; pyridine 2: concentrated H2SO4 View Scheme
参考文献
Jones; Watkinson
Journal of the Chemical Society, 1958 , p. 4064,4068
反应条件
T=150 - 180°C; 0.5 h; Yield given;
参考文献
Davis, Franklin A.; Lamendola, Joseph; Nadir, Upender; Kluger, Edward W.; Sedergran, Thomas C.; et al.
Journal of the American Chemical Society, 1980 , vol. 102, # 6 p. 2000 - 2005
反应条件
1.1: triethylsilyl trifluoromethanesulphonate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere 2.1: sodium hexamethyldisilazane; triethylamine / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere 2.2: 2 h View Scheme
参考文献
Organic and Biomolecular Chemistry, , vol. 9, # 16 p. 5648 - 5651
参考文献
Kariyone; Kimura
Yakugaku Zasshi, 1923 , p. 52
Chem. Zentralbl., 1927 , vol. 98, # I p. 1825
Full Text Show Details
Kariyone; Kimura
Yakugaku Zasshi, 1925 , # 515 p. 1
Chem. Zentralbl., 1927 , vol. 98, # I p. 1825