2-(4-氯苯基)-1,3-二氧戊环合成路线 (共 31 条)
反应条件
hydrogenchloride; hydroxylamine hydrochloride 2 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 41, # 11 p. 2042 - 2043
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy 1.) THF, 63 deg C, 0.5 h; Yield given. Multistep reaction;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4840 - 4844
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy-KI 1.) benzene/THF, 63 deg C, 1.75 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Lourak, Mouhsine; Vanderesse, Regis; Fort, Yves; Caubere, Paul
Journal of Organic Chemistry, 1989 , vol. 54, # 20 p. 4844 - 4848
反应条件
NaH-t-AmONa-Ni(OAc)2-bpy-KI 1.) benzene/THF, 63 deg C, 1.75 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 54, # 20 p. 4844 - 4848
反应条件
hafnium tetrachloride in acetonitrile T=20°C; Strecker Aminoacid Synthesis; 0.5 h; Inert atmosphere;
参考文献
Zhang, Xue-Lin; Wu, Qin-Pei; Zhang, Qing-Shan
Journal of Chemical Research, 2013 , vol. 37, # 11 p. 690 - 693
反应条件
lithium aluminium tetrahydride; (η5-C5H5)titanium trichloride in diethyl ether 12 h; Heating; Title compound not separated from byproducts;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 5 p. 421 - 424
反应条件
lithium aluminium tetrahydride; zirconium tetrachloride in diethyl ether 12 h; Heating; Yield given. Yields of byproduct given;
参考文献
Shaozu, Wu; Tianhui, Ren; Ning, Chen; Yulan, Zhang
Organic Preparations and Procedures International, 1991 , vol. 23, # 4 p. 427 - 431
反应条件
lithium aluminium tetrahydride; (η5-C5H5)titanium trichloride in diethyl ether 12 h; Heating; Title compound not separated from byproducts;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 5 p. 421 - 424
反应条件
cerium trifluoromethanesulfonate in nitromethane; water T=20°C; 2 h;
参考文献
Dalpozzo, Renato; De Nino, Antonio; Maiuolo, Loredana; Procopio, Antonio; Tagarelli, Antonio; Sindona, Giovanni; Bartoli, Giuseppe
Journal of Organic Chemistry, 2002 , vol. 67, # 25 p. 9093 - 9095
反应条件
bismuth trifluoromethanesulphonate in acetonitrile
T=82°C; 8 h; regioselective reaction;
参考文献
Zhang, Xue-Lin; Wu, Qin-Pei; Zhang, Qing-Shan
Journal of Chemical Research, 2013 , vol. 37, # 11 p. 677 - 680