1.1: n-butyllithium / tetrahydrofuran / 0.5 h / -10 °C
1.2: tetrahydrofuran / 0 - 25 °C
2.1: LiAlH4 / diethyl ether / 0.5 h / 0 °C
View Scheme
参考文献
Jones, Graham B.; Wright, Justin M.; Plourde, Gary W.; Hynd, George; Huber, Robert S.; Mathews, Jude E.
Journal of the American Chemical Society, 2000 , vol. 122, # 9 p. 1937 - 1944
tris (triphenylphosphine)rhodium(I) chloride in ethanol
T=60°C; 2 h;
参考文献
Grigg, Ronald; Scott, Ronald; Stevenson, Paul
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1357 - 1364