苯并[b]萘并[2,1-d]呋喃合成路线 （共 14 条）
反应条件
palladium diacetate; potassium carbonate in N,N-dimethyl-formamide T=105°C; 24 h; Schlenk techniqueInert atmosphere; TemperatureConcentration;
参考文献
Motti, Elena; Della Ca, Nicola; Xu, Di; Armani, Simone; Aresta, Brunella Maria; Catellani, Marta
Tetrahedron, 2013 , vol. 69, # 22 p. 4421 - 4428
反应条件
[Rh(acac)(COD)]2; potassium iodide in acetic anhydride T=160°C; 10 h; Inert atmosphere;
参考文献
Maetani, Shinji; Fukuyama, Takahide; Ryu, Ilhyong
Organic Letters, 2013 , vol. 15, # 11 p. 2754 - 2757
反应条件
2Ag(1+)*CH2O3(2-); Pd(TFA)2 in 1,4-dioxane; dimethyl sulfoxide T=150°C; 14 h; Inert atmosphere; regioselective reaction;
参考文献
Wang, Congyang; Piel, Isabel; Glorius, Frank
Journal of the American Chemical Society, 2009 , vol. 131, p. 4194 - 4195
反应条件
[RhCl(η2:η2-cycloocta-1,5-diene)]2; {(S)-1-[(R)-(diphenylphosphino)ferrocenyl]}ethyl-di-tert-butylphosphine; palladium diacetate; caesium carbonate; 2-(dicyclohexylphosphino)-2',4',6'-tri-i-propyl-1,1’-biphenyl in tetrahydrofuran; water T=75°C; 15 h; Inert atmosphereSealed tube;
参考文献
Tsui, Gavin Chit; Tsoung, Jennifer; Dougan, Patrick; Lautens, Mark
Organic Letters, 2012 , vol. 14, # 21 p. 5542 - 5545
反应条件
T=850°C; P=0.001 - 0.1 Torr;
参考文献
Aitken, R. Alan; Burns, Graham; Morrison, John J.
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 23 p. 3937 - 3941
反应条件
T=650°C; P=0.005 Torr; 1 h; Flash vacuum pyrolysis;
参考文献
Black, Michael; Cadogan; McNab, Hamish
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 13 p. 2961 - 2967
反应条件
1: toluene-4-sulfonic acid / toluene / 24 h / Reflux 2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 12 h / Inert atmosphere; Reflux View Scheme
参考文献
Idemitsu Kosan Co., Ltd.; ITO, Hirokatsu; KAWAMURA, Masahiro; KAWAMURA, Yuichiro; MIZUKI, Yumiko; SAITO, Hiroyuki
Patent: EP2644607 A1, 2013 ;
反应条件
1: toluene-4-sulfonic acid / toluene / 24 h / Reflux 2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / 1,4-dioxane / 12 h / Inert atmosphere; Reflux View Scheme
参考文献
Idemitsu Kosan Co., Ltd.; ITO, Hirokatsu; KAWAMURA, Masahiro; KAWAMURA, Yuichiro; MIZUKI, Yumiko; SAITO, Hiroyuki
Patent: EP2644607 A1, 2013 ;
反应条件
1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / methanol; toluene / 24 h / |Reflux 2: boron tribromide / dichloromethane / 0 - 20 °C / |Inert atmosphere 3: water / acetonitrile / 1 h / |Inert atmosphere; |UV-irradiation View Scheme
参考文献
Basaric, Nikola; Doslic, Nacrossed D Signa; Ivkovic, Jakov; Wang, Yu-Hsuan; Veljkovic, Jelena; Mlinaric-Majerski, Kata; Wan, Peter
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1811 - 1823
反应条件
water in acetonitrile 1 h; Inert atmosphereUV-irradiation;
参考文献
Basaric, Nikola; Doslic, Nacrossed D Signa; Ivkovic, Jakov; Wang, Yu-Hsuan; Veljkovic, Jelena; Mlinaric-Majerski, Kata; Wan, Peter
Journal of Organic Chemistry, 2013 , vol. 78, # 5 p. 1811 - 1823
