1-氯-3-(苯磺酰基)丙酮合成路线 （共 9 条）
反应条件
1: 46 percent / pyridine / 3 h / 5 °C 2: 65 percent / AcONa / tetrahydrofuran; H2O / 6 h / Heating 3: 65 percent / pyridine; H2O / 3 h / 5 °C View Scheme
参考文献
Takahashi, Masahiko; Oshida, Takeshi
Journal of Heterocyclic Chemistry, 1992 , vol. 29, # 2 p. 543 - 545
反应条件
tetra-(n-butyl)ammonium iodide; potassium iodide in N,N-dimethyl-formamide
T=20°C; 6 h;
参考文献
Chen, Yu; Lam, Yulin; Lai, Yee-Hing
Organic Letters, 2002 , vol. 4, # 22 p. 3935 - 3937
反应条件
tetra(n-butyl)ammonium hydrogensulfate in acetonitrile
T=20°C; 12 h;
参考文献
Chen, Yu; Lam, Yulin; Lai, Yee-Hing
Organic Letters, 2002 , vol. 4, # 22 p. 3935 - 3937
反应条件
3-chloro-benzenecarboperoxoic acid in chloroform
30 h; Ambient temperature; Yield given;
参考文献
Tanikaga, Rikuhei; Hosoya, Ken; Kaji, Aritsune
Synthesis, 1987 , # 4 p. 389 - 390
反应条件
sulfuryl dichloride in dichloromethane; acetic acid
T=25°C; 4 h; Yield given;
参考文献
Grosset, Stuart J.; Dubey, Pramod K.; Gill, Glen H.; Cameron, Stanley T.; Gardner, Patrick A.
Canadian Journal of Chemistry, 1984 , vol. 62, p. 798 - 807
反应条件
1: 80 percent / methanol; H2O / 1.) 0 deg C, 7 h, 2.) room temp., 10 h
2: m-chloroperbenzoic acid / CHCl3 / 30 h / Ambient temperature
View Scheme
参考文献
Tanikaga, Rikuhei; Hosoya, Ken; Kaji, Aritsune
Synthesis, 1987 , # 4 p. 389 - 390
反应条件
1: 80 percent / NaOH / H2O; methanol / 0 deg C, 7 h then r.t. 10 h
2: MCPBA / CHCl3 / 30 h / Ambient temperature
View Scheme
参考文献
Tanikaga, Rikuhei; Hosoya, Ken; Kaji, Aritsune
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1799 - 1804
反应条件
1: ethanol / Heating
2: sulfuryl chloride / CH2Cl2; acetic acid / 4 h / 25 °C
View Scheme
参考文献
Grosset, Stuart J.; Dubey, Pramod K.; Gill, Glen H.; Cameron, Stanley T.; Gardner, Patrick A.
Canadian Journal of Chemistry, 1984 , vol. 62, p. 798 - 807
反应条件
1: 1.) baker's yeast, 2.) Ag2O
2: 100 percent / base / tetrahydrofuran / Ambient temperature
View Scheme
参考文献
Tanikaga, Rikuhei; Hosoya, Ken; Kaji, Aritsune
Journal of the Chemical Society, Chemical Communications, 1986 , # 11 p. 836 - 837
