Maire, J. C.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1959 , vol. 249, p. 1359 - 1360
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Gmelin Handbook: Sn: Org.Verb.1, 1.1.1.2.1, page 57 - 62
1: ethyl magnesium chloride With titanium(IV) isopropylate in dichloromethane T=-78°C; 0.166667 h; Inert atmosphere; 2: benzaldehyde With (R)-3-(3,5-diphenylphenyl)-2,2'-dihydroxy-1,1'-binaphthyl in diethyl ether; dichloromethane T=0°C; 3 h; Inert atmosphere; 3: With hydrogenchloride; water in diethyl ether; dichloromethane T=0°C; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
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Bulletin of the Chemical Society of Japan, , vol. 83, # 1 p. 19 - 32
1: With trans-N,N′-bis(2-pyridinylmethylene)-1,2-cyclohexanediamine; iron(II) chloride in tetrahydrofuran T=-78°C; 0.25 h; 2: With NaBEt3H in tetrahydrofuran T=-78 - 20°C; 16 h;
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Le Bailly, Bryden A. F.; Greenhalgh, Mark D.; Thomas, Stephen P.
Chemical Communications, 2012 , vol. 48, # 10 p. 1580 - 1582
1: With iron (+/-)-(N,N'-bis(pyridin-2-ylmethylene)cyclohexane-1,2-diamine)dichloride in tetrahydrofuran T=-20°C; 0.25 h; 2: With LiH3BNMe2 in tetrahydrofuran T=-20 - 20°C; 16 h;
参考文献
Le Bailly, Bryden A. F.; Greenhalgh, Mark D.; Thomas, Stephen P.
Chemical Communications, 2012 , vol. 48, # 10 p. 1580 - 1582
1: With iron (+/-)-(N,N'-bis(pyridin-2-ylmethylene)cyclohexane-1,2-diamine)dichloride in tetrahydrofuran T=-20°C; 0.25 h; 2: With sodium tetrahydroborate in tetrahydrofuran T=-20 - 20°C; 16 h;
参考文献
Le Bailly, Bryden A. F.; Greenhalgh, Mark D.; Thomas, Stephen P.
Chemical Communications, 2012 , vol. 48, # 10 p. 1580 - 1582
