1-(3-苯基氨基苯基)-乙酮合成路线 （共 10 条）
反应条件
potassium carbonate in water T=20°C;
参考文献
Sawant, Sanghapal D.; Srinivas, Mahesuni; Aravinda Kumar; Lakshma Reddy; Singh, Parvinder Pal; Singh, Baldev; Sharma, Amit Kumar; Sharma; Vishwakarma, Ram A.
Tetrahedron Letters, 2013 , vol. 54, # 39 p. 5351 - 5354
反应条件
potassium phosphate; N-[2'-(dicyclohexylphosphino)-1,1'-biphenyl-2-yl]-N,N-dimethylamine; tris(dibenzylideneacetone)dipalladium (0) in ethylene glycol dimethyl ether T=100°C; Arylation; 22 h;
参考文献
Wolfe, John P.; Tomori, Hiroshi; Sadighi, Joseph P.; Yin, Jingjun; Buchwald, Stephen L.
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 1158 - 1174
反应条件
tris(dibenzylideneacetone)dipalladium (0); 2,4,6-(i-Pr)3-[2-P(t-Bu)2-phenyl]benzene; 1,8-diazabicyclo[5.4.0]undec-7-ene in toluene T=125°C; 0.5 h; microwave irradiation;
参考文献
Tundel, Rachel E.; Anderson, Kevin W.; Buchwald, Stephen L.
Journal of Organic Chemistry, 2006 , vol. 71, # 1 p. 430 - 433
反应条件
pyridine; copper diacetate in dichloromethane T=20°C;
参考文献
Greenbaum, Doron C.; Mackey, Zachary; Hansell, Elizabeth; Doyle, Patricia; Gut, Jiri; Caffrey, Conor R.; Lehrman, Julia; Rosenthal, Philip J.; McKerrow, James H.; Chibale, Kelly
Journal of Medicinal Chemistry, 2004 , vol. 47, # 12 p. 3212 - 3219
反应条件
sodium t-butanolate; [Na2PdCl4]; dicyclohexyl-(9-ethyl-9H-fluoren-9-yl)phosphane*HBF4 in toluene T=120°C; Buchwald-Hartwig coupling reaction; 3 h;
参考文献
Fleckenstein, Christoph A.; Plenio, Herbert
Chemistry - A European Journal, 2007 , vol. 13, # 9 p. 2701 - 2716
反应条件
1: K2CO3, Cu, CuI / 3-methyl-butan-1-ol / Heating 2: (decarboxylation) View Scheme
参考文献
Itier,J.; Casadevall,A.
Bulletin de la Societe Chimique de France, 1969 , p. 2342 - 2355
反应条件
1: K2CO3, Cu, CuI / 3-methyl-butan-1-ol / Heating 2: (decarboxylation) View Scheme
参考文献
Itier,J.; Casadevall,A.
Bulletin de la Societe Chimique de France, 1969 , p. 2342 - 2355
参考文献
Itier,J.; Casadevall,A.
Bulletin de la Societe Chimique de France, 1969 , p. 2342 - 2355
反应条件
1: copper; isoamyl alcohol 2: 250 °C View Scheme
参考文献
Elson; Gibson
Journal of the Chemical Society, 1931 , p. 2381,2386
反应条件
1: copper; isoamyl alcohol 2: 250 °C View Scheme
参考文献
Elson; Gibson
Journal of the Chemical Society, 1931 , p. 2381,2386
