(1,3,3,3-四氯丙基)苯合成路线 (共 21 条)
反应条件
N-dodecane; [RuH(η5-[9-SMe2-7,8-C2B9H10])(PPh3)2] in toluene T=40°C; Kharash addition; 16 h;
参考文献
Tutusaus, Oscar; Delfosse, Sebastien; Demonceau, Albert; Noels, Alfred F.; Vinas, Clara; Teixidor, Francesc
Tetrahedron Letters, 2003 , vol. 44, # 46 p. 8421 - 8425
反应条件
Ru2Cl4((-)-diop)3 in benzene T=100°C;
参考文献
Kameyama, Masayuki; Kamigata, Nobumasa
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 10 p. 3687 - 3692
反应条件
Ru2Cl4((+)-diop)3 T=100°C; various reagents; further styrene derivatives; Product distribution;
参考文献
Kameyama, Masayuki; Kamigata, Nobumasa
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 10 p. 3687 - 3692
反应条件
iron in N,N-dimethyl-formamide T=60°C; 5 h;
参考文献
Dneprovskii; Kasatochkin
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 10 p. 1444 - 1450
反应条件
anhydrous diethylamine hydrochloride; CuCl2*2H2O T=100°C; 9 h;
参考文献
Asscher,M.; Vofsi,D.
Journal of the Chemical Society, 1963 , p. 1887 - 1896
反应条件
N,N-dimethyl-formamide; pentacarbonyliron(0)
参考文献
Velichko,F.K.; Vinogradova,L.V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1978 , vol. 27, p. 204 - 206
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1978 , vol. 27, p. 232 - 234
反应条件
RuCl2(p-cymene)(N,N-dimesyl-4,5-dichloroimidazole) in N-dodecane; toluene T=90°C; 10 h; Product distributionKinetics; Further Variations:CatalystsTemperaturesreactant ratios, reaction times;
参考文献
Richel, Aurore; Delfosse, Sebastien; Cremasco, Cedric; Delaude, Lionel; Demonceau, Albert; Noels, Alfred F.
Tetrahedron Letters, 2003 , vol. 44, # 32 p. 6011 - 6015
反应条件
potassium hydroxide in ethanol 18 h; Heating; Further byproducts given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 56, # 6 p. 1795 - 1798
反应条件
1: 22 percent / EtONa / 18 h / Heating 2: 18 percent / EtONa / ethanol / 18 h / 80 °C View Scheme
参考文献
Akiyama, Takeo; Yoshida, Yasuki; Hanawa, Tokiko; Sugimori, Akira
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 6 p. 1795 - 1798
反应条件
sodium ethanolate 18 h; Heating; Further byproducts given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 56, # 6 p. 1795 - 1798