反式-2-苯基-1-环已醇合成路线 (共 72 条)
反应条件
boron trifluoride diethyl etherate in tetrahydrofuran; hexane T=-78°C; 0.166667 h;
参考文献
Eis, Michael J.; Wrobel, J. E.; Ganem, Bruce
Journal of the American Chemical Society, 1984 , vol. 106, p. 3693 - 3694
反应条件
1: With borane-THF T=0°C; 2: With dihydrogen peroxide; sodium hydroxide in water
参考文献
Younai, Ashkaan; Fettinger, James C.; Shaw, Jared T.
Tetrahedron, 2012 , vol. 68, # 22 p. 4320 - 4327
反应条件
copper(l) iodide in tetrahydrofuran; diethyl ether T=20°C; 7 h;
参考文献
Gonzalez-Sabin, Javier; Gotor, Vicente; Rebolledo, Francisca
Tetrahedron Asymmetry, 2005 , vol. 16, # 18 p. 3070 - 3076
反应条件
boron trifluoride; lithium bromide in diethyl ether T=-78 - -50°C; 1 h;
参考文献
Alexakis, A.; Jachiet, D.; Normant, J. F.
Tetrahedron, 1986 , vol. 42, # 20 p. 5607 - 5620
反应条件
1,4-dioxane; nickel T=160°C; P=73550.8 - 147102 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 60, p. 664,666
反应条件
sodium amalgam; ethanol
参考文献
Journal of the American Chemical Society, , vol. 62, p. 1159
反应条件
N,N'-dimethyl-N,N'-propyleneurea; anhydrous 4,4'-bipyridyl; bis(cyclopentadienyl)titanium dichloride; manganese; NiCl2*0.97C2H6O; triethyl amine hydrochloride T=20°C; 12 h; Inert atmosphereGlovebox;
参考文献
Zhao, Yang; Weix, Daniel J.
Journal of the American Chemical Society, 2014 , vol. 136, # 1 p. 48 - 51
反应条件
1: With hydrogen in methanol T=70 - 75°C; P=30003 Torr; 5.5 h; Autoclave; 2: With dimethyl sulfoxide 0.5 h; RefluxInert atmosphere;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 46 p. 8082 - 8091
反应条件
hydrogen in methanol T=70 - 75°C; P=30003 Torr; 5.5 h; Autoclave;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 46 p. 8082 - 8091
反应条件
sodium tetrahydroborate; titanium tetrachloride in ethylene glycol dimethyl ether Ambient temperature;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 9 p. 414 - 415