2-甲氧基-1,4-萘醌合成路线 (共 80 条)
反应条件
sodium acetate; manganese triacetate in acetic acid
T=80°C; 4 h; various aromatics; other malonates; different temperatures; different time; Product distributionMechanism;
参考文献
Citterio, Attilio; Santi, Roberto; Fiorani, Tiziana; Strologo, Sauro
Journal of Organic Chemistry, 1989 , vol. 54, # 11 p. 2703 - 2712
反应条件
sodium acetate; manganese triacetate
T=80°C; 6 h; also without CH3COONa; further times, Mn(III) oxidants, alkoxynaphthalenes; also with acetylacetone, ethyl acetoacetate, ethyl cyanoacetate, acetone; Product distributionMechanism;
参考文献
Citterio, Attilio; Fancelli, Daniele; Santi, Roberto; Pagani, Anselmo; Bonsignore, Stefano
Gazzetta Chimica Italiana, 1988 , vol. 118, # 5 p. 405 - 408
参考文献
Moubasher et al.
Journal of the Chemical Society, 1950 , p. 1998
Full Text Show Details
Eistert; Mueller
Chemische Berichte, 1959 , vol. 92, p. 2071,2073
反应条件
boron trifluoride diethyl etherate in dichloromethane
-78 deg C to -50 deg C;
参考文献
Naruta, Yoshinori
Journal of the American Chemical Society, 1980 , vol. 102, # 11 p. 3774 - 3783
反应条件
in N,N-dimethyl-formamide
T=-23°C; 3 h;
参考文献
Araki, Shuki; Katsumura, Nobuhito; Butsugan, Yasuo
Journal of Organometallic Chemistry, 1991 , vol. 415, # 1 p. 7 - 24
反应条件
zinc in tetrahydrofuran
24 h; Further byproducts given;
参考文献
Kapoor, N. K.; Gupta, R. B.; Khanna, R. N.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1982 , vol. 21, # 3 p. 189 - 191
参考文献
Fieser et al.
Journal of the American Chemical Society, 1948 , vol. 70, p. 3177
反应条件
MgCl2*6H2O; toluene-4-sulfonic acid in methanol
10 h; Reflux;
参考文献
Francisco, Acacio I.; Vargas, Maria D.; Carneiro, J. Walkimar de M.; Lanznaster, Mauricio; Torres, Jose C.; Camara, Celso A.; Pinto, Angelo C.
Journal of Molecular Structure, 2008 , vol. 891, # 1-3 p. 228 - 232
反应条件
in ethanol; dichloromethane
2 h; Ambient temperature;
参考文献
Kallmayer; Seyfang
Archiv der Pharmazie, 1980 , vol. 313, # 7 p. 603 - 611
反应条件
MgCl2*6H2O; toluene-4-sulfonic acid in methanol
6 h; Reflux;
参考文献
Francisco, Acacio I.; Vargas, Maria D.; Carneiro, J. Walkimar de M.; Lanznaster, Mauricio; Torres, Jose C.; Camara, Celso A.; Pinto, Angelo C.
Journal of Molecular Structure, 2008 , vol. 891, # 1-3 p. 228 - 232