反应条件
1: 3-Butynoic acid With 2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in toluene T=100°C; 3 h; 2: n-pentylcarbonyl chloride With tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=50°C; Stille reaction; 6 h; Further stages.;
参考文献
Thibonnet, Jerome; Abarbri, Mohamed; Parrain, Jean-Luc; Duchene, Alain
The Journal of organic chemistry, 2002 , vol. 67, # 11 p. 3941 - 3944
