1-苯基-1,2-环氧丙烷合成路线 (共 29 条)
反应条件
lithium diisopropyl amide
参考文献
Journal of the Chemical Society, Chemical Communications, , # 16 p. 1238 - 1240
反应条件
bis-[(trifluoroacetoxy)iodo]benzene in dichloromethane 24 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 46, p. 5231 - 5233
反应条件
(R,R)-(salen)Cr(III)-Cl in dichloromethane T=0°C; 48 h;
参考文献
Kureshy, Rukhsana Ilays; Prathap, K. Jeya; Kumar, Manish; Bera, Prasanta Kumar; Khan, Noor-Ul Hasan; Abdi, Sayed Hasan Razi; Bajaj, Hari Chandra
Tetrahedron, 2011 , vol. 67, # 43 p. 8300 - 8307
反应条件
chiral polymer-based chromium salen in dichloromethane T=-10°C; 36 h; Title compound not separated from byproducts;
参考文献
Kureshy, Rukhsana Ilays; Prathap, K. Jeya; Kumar, Manish; Bera, Prasanta Kumar; Khan, Noor-Ul Hasan; Abdi, Sayed Hasan Razi; Bajaj, Hari Chandra
Tetrahedron, 2011 , vol. 67, # 43 p. 8300 - 8307
反应条件
C68H92Cr2N8O4(2+)*2Cl(1-) in methanol; dichloromethane T=20°C; 30 h; optical yield given as percent eeenantioselective reaction;
参考文献
Kureshy, Rukhsana Ilays; Prathap, K. Jeya; Kumar, Manish; Bera, Prasanta Kumar; Khan, Noor-Ul Hasan; Abdi, Sayed Hasan Razi; Bajaj, Hari Chandra
Tetrahedron, 2011 , vol. 67, # 43 p. 8300 - 8307
反应条件
C68H92Cr2N8O4(2+)*2Cl(1-) in methanol; dichloromethane T=20°C; 20 h; optical yield given as percent eeenantioselective reaction;
参考文献
Kureshy, Rukhsana Ilays; Prathap, K. Jeya; Kumar, Manish; Bera, Prasanta Kumar; Khan, Noor-Ul Hasan; Abdi, Sayed Hasan Razi; Bajaj, Hari Chandra
Tetrahedron, 2011 , vol. 67, # 43 p. 8300 - 8307
反应条件
C68H92Cr2N8O4(2+)*2Cl(1-) in methanol; dichloromethane T=20°C; 24 h; optical yield given as percent eeenantioselective reaction;
参考文献
Kureshy, Rukhsana Ilays; Prathap, K. Jeya; Kumar, Manish; Bera, Prasanta Kumar; Khan, Noor-Ul Hasan; Abdi, Sayed Hasan Razi; Bajaj, Hari Chandra
Tetrahedron, 2011 , vol. 67, # 43 p. 8300 - 8307
反应条件
(R,R)-[Cr(salen)] hexafluoroantimonate; 4 A molecular sieve; tert-butyl alcohol in various solvent(s) T=0°C; 36 h; Title compound not separated from byproducts;
参考文献
Bandini, Marco; Cozzi, Pier Giorgio; Melchiorre, Paolo; Umani-Ronchi, Achille
Angewandte Chemie - International Edition, 2004 , vol. 43, # 1 p. 84 - 87
反应条件
chiral polymer-based chromium salen in dichloromethane T=20°C; 12 h; Title compound not separated from byproducts;
参考文献
Kureshy, Rukhsana I.; Singh, Surendra; Khan, Noor-ul H.; Abdi, Sayed H.R.; Agrawal, Santosh; Jasra, Raksh V.
Tetrahedron Asymmetry, 2006 , vol. 17, # 11 p. 1638 - 1643
反应条件
palladium 10 on activated carbon; hydrogen in methanol T=20°C; P=760.051 Torr; 2 h; regioselective reaction;
参考文献
Blasio, Nadia Di; Lopardo, Maria Teresa; Lupattelli, Paolo
European Journal of Organic Chemistry, 2009 , # 6 p. 938 - 944