4-(1H-吡咯-1-基)苯甲腈合成路线 (共 6 条)
反应条件
in acetic acid 0.5 h; Heating;
参考文献
Kaugars, Girts; Watt, William
Journal of Heterocyclic Chemistry, 1993 , vol. 30, # 2 p. 497 - 500
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; caesium carbonate in toluene T=100°C; 12 h;
参考文献
Journal of the American Chemical Society, , vol. 120, # 4 p. 827 - 828
反应条件
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0) in acetonitrile Substitution; 1 h; Heating;
参考文献
Anderson, Benjamin A.; Bell, Edward C.; Ginah, Francis O.; Harn, Nancy K.; Pagh, Lisa M.; Wepsiec, James P.
Journal of Organic Chemistry, 1998 , vol. 63, # 23 p. 8224 - 8228
反应条件
trimethylsilylazide; silver carbonate in dimethyl sulfoxide T=100°C; 12 h;
参考文献
Shen, Tao; Wang, Teng; Qin, Chong; Jiao, Ning
Angewandte Chemie - International Edition, 2013 , vol. 52, # 26 p. 6677 - 6680
Angew. Chem., 2013 , vol. 125, # 26 p. 6809 - 6612,4
反应条件
1: N,N-dimethyl-formamide With trichlorophosphate T=0°C; Vilsmeier Reaction; 2: 4-(1H-pyrrol-1-yl)benzonitrile in 1,2-dichloro-ethane T=0 - 20°C; Vilsmeier Reaction; 7 h;
参考文献
Li, Huiyang; Yang, Luying; Tang, Runli; Hou, Yingqin; Yang, Yizhou; Wang, Heng; Han, Hongwei; Qin, Jingui; Li, Qianqian; Li, Zhen
Dyes and Pigments, 2013 , vol. 99, # 3 p. 863 - 870
反应条件
nickel monoaluminide in pyridine; ethyl acetate
参考文献
Merck and Co., Inc.
Patent: US4207329 A1, 1980 ;