苯并[e][1]苯并呋喃合成路线 （共 30 条）
反应条件
magnesium in methanol
Ambient temperature;
参考文献
Neo, Ana G.; Lopez, Carmen; Romero, Victor; Antelo, Berta; Delamano, Jose; Perez, Antonio; Fernandez, Dolores; Almeida, Jesus F.; Castedo, Luis; Tojo, Gabriel
Journal of Organic Chemistry, 2010 , vol. 75, # 20 p. 6764 - 6770
反应条件
T=600°C; P=0.1 Torr; flash vacuum pyrolysis;
参考文献
Hussain, Amjad; Parrick, John
Tetrahedron Letters, 1983 , vol. 24, # 6 p. 609 - 612
反应条件
in chloroform
T=60°C; Isomerization; Michael addition; rearrangement; cyclization; 72 h;
参考文献
Haselgrove, Thomas D.; Jevric, Martyn; Taylor, Dennis K.; Tiekink, Edward R. T.
Tetrahedron, 1999 , vol. 55, # 51 p. 14739 - 14762
反应条件
T=650°C; P=0.001 - 0.01 Torr;
参考文献
Black, Michael; Cadogan, J. I. G.; Cartwright, Gary A.; McNab, Hamish; MacPherson, Andrew D.
Journal of the Chemical Society, Chemical Communications, 1993 , # 11 p. 959 - 960
反应条件
T=650°C; P=0.002 Torr; 0.333333 h;
参考文献
Black, Michael; Cadogan; McNab, Hamish; MacPherson, Andrew D.; Roddam, V. Peter; Smith, Carol; Swenson, Helen R.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 17 p. 2483 - 2493
反应条件
1: 50 percent Turnov. / oxygen; Rose Bengal, bis(triethylammonium)salt / CH2Cl2 / 5 h / 5 - 10 °C / Irradiation
2: 15 mg / Et3N / CHCl3 / 5 °C
View Scheme
参考文献
Haselgrove, Thomas D.; Jevric, Martyn; Taylor, Dennis K.; Tiekink, Edward R. T.
Tetrahedron, 1999 , vol. 55, # 51 p. 14739 - 14762
反应条件
1: 71 percent
2: 50 percent Turnov. / oxygen; Rose Bengal, bis(triethylammonium)salt / CH2Cl2 / 5 h / 5 - 10 °C / Irradiation
3: 15 mg / Et3N / CHCl3 / 5 °C
View Scheme
参考文献
Haselgrove, Thomas D.; Jevric, Martyn; Taylor, Dennis K.; Tiekink, Edward R. T.
Tetrahedron, 1999 , vol. 55, # 51 p. 14739 - 14762
反应条件
T=610°C; P=0.05 - 0.1 Torr;
参考文献
Engler, T. A.; Shechter, H.
Tetrahedron Letters, 1982 , vol. 23, # 27 p. 2715 - 2718
反应条件
1: 41 percent / K2CO3 / acetone / 2 h / 60 °C
2: [RuClH(CO)(PPh3)3] / toluene / 4 h / 80 °C
3: 0.030 g / ((Mes)2C3H5N2)Cl2Ru=CHPh / toluene / 12 h / 80 °C
View Scheme
参考文献
Van Otterlo, Willem A.L.; Morgans, Garreth L.; Madeley, Lee G.; Kuzvidza, Samuel; Moleele, Simon S.; Thornton, Natalie; De Koning, Charles B.
Tetrahedron, 2005 , vol. 61, # 32 p. 7746 - 7755
反应条件
1: [RuClH(CO)(PPh3)3] / toluene / 4 h / 80 °C
2: 0.030 g / ((Mes)2C3H5N2)Cl2Ru=CHPh / toluene / 12 h / 80 °C
View Scheme
参考文献
Van Otterlo, Willem A.L.; Morgans, Garreth L.; Madeley, Lee G.; Kuzvidza, Samuel; Moleele, Simon S.; Thornton, Natalie; De Koning, Charles B.
Tetrahedron, 2005 , vol. 61, # 32 p. 7746 - 7755
