N,N-二甲基-2-(三甲基甲硅烷基)乙酰胺合成路线 （共 15 条）
反应条件
n-butyllithium; diisopropylamine in tetrahydrofuran; hexane T=-78°C; 2 h;
参考文献
Urayama, Shin'ichi; Inoue, Sumie; Sato, Yoshiro
Journal of Organometallic Chemistry, 1988 , vol. 354, p. 155 - 160
参考文献
Nikolaeva, S. N.; Zolotareva, A. S.; Ponomarev, S. V.; Petrosyan, V. S.
Russian Chemical Bulletin, 1994 , vol. 43, # 5 p. 857 - 861
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1994 , # 5 p. 911 - 915
反应条件
trimethylsilyl bromide
参考文献
Kostyuk,A.S. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1970 , vol. 40, p. 626 - 636,598 - 606
Full Text Show Details
Lutsenko,I.F. et al.
Journal of Organometallic Chemistry, 1969 , vol. 17, p. 241 - 262
参考文献
Lutsenko,I.F. et al.
Journal of Organometallic Chemistry, 1969 , vol. 17, p. 241 - 262
参考文献
Arai, Shigeru; Sakurai, Takuya; Asakura, Hitomi; Fuma, Shin-Ya; Shioiri, Takayuki; Aoyama, Toyohiko
Heterocycles, 2001 , vol. 55, # 12 p. 2283 - 2287
反应条件
methanol 1.) dibutyl ether, 80 deg C, 8 h, 2.) Et2O; Yield given. Multistep reaction;
参考文献
Nikolaeva, S. N.; Zolotareva, A. S.; Ponomarev, S. V.; Petrosyan, V. S.
Russian Chemical Bulletin, 1994 , vol. 43, # 5 p. 857 - 861
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1994 , # 5 p. 911 - 915
反应条件
2: 140 °C View Scheme
参考文献
Lutsenko,I.F. et al.
Journal of Organometallic Chemistry, 1969 , vol. 17, p. 241 - 262
参考文献
Pellon, Pascal; Hamelin, Jack
Tetrahedron Letters, 1986 , vol. 27, # 46 p. 5611 - 5614
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Laws, David D.; Wishart, David S.; Havlin, Robert H.; Westmeyer, Mark; Sykes, Brian D.; Oldfield, Eric
Journal of Magnetic Resonance, Series B, 1995 , vol. 108, # 3 p. 274 - 275
反应条件
1: With C{N(2,6-iPr2C6H3)CH}2 in N,N-dimethyl-formamide T=0 - 20°C; Reformatsky Reaction; Inert atmosphereGreen chemistry; 2: With hydrogenchloride in water; N,N-dimethyl-formamide Reformatsky Reaction; 0.5 h; Inert atmosphereGreen chemistry;
参考文献
Zou, Xiao-Lei; Du, Guang-Fen; Sun, Wan-Fu; He, Lin; Ma, Xiao-Wei; Gu, Cheng-Zhi; Dai, Bin
Tetrahedron, 2013 , vol. 69, # 2 p. 607 - 612
