5-氯-2-甲氧基苯磺酰氯合成路线 (共 6 条)
反应条件
chlorosulfonic acid 3 h; Ambient temperature;
参考文献
Guo, Cheng; Qiu, Jun; Zhang, Xumu; Verdugo, Dawn; Larter, Martin L.; Christie, Ray; Kenney, Patrick; Walsh, Patrick J.
Tetrahedron, 1997 , vol. 53, # 12 p. 4145 - 4158
反应条件
1: K2CO3 / acetone 2: 74 percent / ClSO3H / 3 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 53, # 12 p. 4145 - 4158
参考文献
Journal of the Chemical Society, , vol. 127, p. 2746
参考文献
Journal of the Chemical Society, , vol. 127, p. 2746
反应条件
1: 77 percent / triethylamine / diethyl ether; ethanol / 0.75 h / Heating
2: 82 percent / Na2CO3 / acetone / 8 h / Heating
View Scheme
参考文献
Fournier; Moreau; Narcisse; Choay
European Journal of Medicinal Chemistry, 1982 , vol. 17, # 1 p. 81 - 84