1,3-双(氯二甲基甲硅烷基)丙烷合成路线 （共 9 条）
反应条件
chloro-trimethyl-silane; aluminium trichloride
参考文献
Hosomi, Akira; Kohra, Shinya; Tominaga, Yoshinori; Inaba, Masahiro; Sakurai, Hideki
Chemical & Pharmaceutical Bulletin, 1988 , vol. 36, p. 2342 - 2345
反应条件
N-chloro-succinimide in tetrachloromethane Heating;
参考文献
Weyenberg,D.R.; Nelson,L.E.
Journal of Organic Chemistry, 1965 , vol. 30, p. 2618 - 2621
反应条件
1: H2PtCl6 / propan-2-ol 2: N-chloro-succinimide / CCl4 / Heating View Scheme
参考文献
Weyenberg,D.R.; Nelson,L.E.
Journal of Organic Chemistry, 1965 , vol. 30, p. 2618 - 2621
反应条件
dihydrogen hexachloroplatinate in isopropyl alcohol Heating;
参考文献
Tacke; Linoh; Attar Bashi; et al.
1982 , vol. 37, # 11 p. 1461 - 1471
反应条件
1: H2PtCl6 2: chlorotrimethylsilane, AlCl3 View Scheme
参考文献
Suzuki, Masato; Obayashi, Tatsuhiko; Saegusa, Takeo
Journal of the Chemical Society, Chemical Communications, 1993 , # 8 p. 717 - 718
反应条件
Ph3SiLi; lithium in tetrahydrofuran
T=15°C; 5 h; Yield given. Yields of byproduct given;
参考文献
Ishikawa, Mitsuo; Yamanaka, Toru; Kumada, Makoto
Journal of Organometallic Chemistry, 1985 , vol. 292, p. 167 - 176
反应条件
Ph3SiLi; lithium in tetrahydrofuran
T=50 - 60°C; 7 h; Yield given. Yields of byproduct given;
参考文献
Ishikawa, Mitsuo; Yamanaka, Toru; Kumada, Makoto
Journal of Organometallic Chemistry, 1985 , vol. 292, p. 167 - 176
参考文献
Marciniec, Bogdan; Malecka, Ewa; Scibiorek, Marek
Macromolecules, 2003 , vol. 36, # 15 p. 5545 - 5550
反应条件
magnesium
1.) THF, 2.) ether, THF, 4 h, reflux; Yield given. Multistep reaction;
参考文献
Tacke; Linoh; Attar Bashi; et al.
1982 , vol. 37, # 11 p. 1461 - 1471
