(8CI,9CI)-四甲基嘧啶合成路线 （共 9 条）
反应条件
trifluoromethylsulfonic anhydride in dichloromethane 24 h; Ambient temperature;
参考文献
Martinez, A. Garcia; Fernandez, A. Herrera; Jimenez, F. Moreno; Fraile, A. Garcia; Subramanian, L. R.; Hanack, M.
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1627 - 1630
反应条件
in acetonitrile-D3 T=-40°C; Photolysis;
参考文献
Banert, Klaus; Koehler, Frank
Angewandte Chemie, International Edition, 2001 , vol. 40, # 1 p. 174 - 177
Angewandte Chemie, 2001 , vol. 113, p. 173 - 176
反应条件
1: 14 percent / tributylhexadecylphosphonium azide / benzene / 80 °C 2: CDCl3 / -60 °C / Photolysis 3: AgBF4 / -25 °C View Scheme
参考文献
Banert, Klaus; Koehler, Frank
Angewandte Chemie, International Edition, 2001 , vol. 40, # 1 p. 174 - 177
Angewandte Chemie, 2001 , vol. 113, p. 173 - 176
反应条件
1: CDCl3 / -60 °C / Photolysis 2: AgBF4 / -25 °C View Scheme
参考文献
Banert, Klaus; Koehler, Frank
Angewandte Chemie, International Edition, 2001 , vol. 40, # 1 p. 174 - 177
Angewandte Chemie, 2001 , vol. 113, p. 173 - 176
反应条件
silver tetrafluoroborate T=-25°C;
参考文献
Banert, Klaus; Koehler, Frank
Angewandte Chemie, International Edition, 2001 , vol. 40, # 1 p. 174 - 177
Angewandte Chemie, 2001 , vol. 113, p. 173 - 176
反应条件
phosphorus pentoxide in decalin 10 h; Heating; Yield given. Yields of byproduct given;
参考文献
Zielinski, W.; Mazik, M.
Polish Journal of Chemistry, 1992 , vol. 66, # 7 p. 1113 - 1119
反应条件
in acetonitrile-D3 T=-40°C; Photolysis;
参考文献
Banert, Klaus; Grimme, Stefan; Herges, Rainer; Hess, Kirsten; Koehler, Frank; Mueck-Lichtenfeld, Christian; Wuerthwein, Ernst-Ulrich
Chemistry - A European Journal, 2006 , vol. 12, # 28 p. 7467 - 7481
参考文献
Roberts
Journal of the Chemical Society, 1952 , p. 3065,3066
反应条件
phosphorus pentoxide in decalin 10 h; Heatingother N-vinylimidoyl chlorides and acetylene derivatives; Mechanism;
参考文献
Zielinski, W.; Mazik, M.
Polish Journal of Chemistry, 1992 , vol. 66, # 7 p. 1113 - 1119
