4-杂氮三环[4.3.1.13,8]十一烷-5-酮合成路线 (共 21 条)
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene RefluxInert atmosphereUV-irradiation;
参考文献
Journal of Organic Chemistry, , vol. 75, # 8 p. 2610 - 2618
反应条件
in dichloromethane T=-78°C; UV-irradiationInert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 75, # 8 p. 2610 - 2618
反应条件
hydrogenchloride; hydroxylamine hydrochloride 0.5 h; Heating;
参考文献
Collection of Czechoslovak Chemical Communications, , vol. 49, # 8 p. 1774 - 1779
反应条件
sodium azide in acetic acid 1 h; Ambient temperature; MechanismProduct distribution;
参考文献
Tetrahedron, , vol. 41, # 18 p. 3753 - 3762
反应条件
hydroxylamine-o-sulphonic acid in diethyl ether; water 0.166667 h; Ambient temperature; Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 17, # 12 p. 2284 - 2289
Zhurnal Organicheskoi Khimii, , vol. 17, # 12 p. 2558 - 2564
反应条件
hydroxylamine-o-sulphonic acid in water Product distribution;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 17, # 12 p. 2284 - 2289
Zhurnal Organicheskoi Khimii, , vol. 17, # 12 p. 2558 - 2564
反应条件
sodium azide 1 h; Ambient temperature; MechanismProduct distribution;
参考文献
Tetrahedron, , vol. 41, # 18 p. 3753 - 3762
反应条件
hydrogenchloride 18 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 48, # 20 p. 3569 - 3571
反应条件
lithium aluminium tetrahydride in diethyl ether
6 h; Heating;
参考文献
St. Georgiev; Saeva; Kinsolving
Journal of Heterocyclic Chemistry, 1986 , vol. 23, # 4 p. 1023 - 1025
参考文献
Pennwalt Corporation
Patent: US4557865 A1, 1985 ;