(S)-(+)-1,2-异亚丙基甘油合成路线 （共 82 条）
反应条件
phosphate buffer; Genzyme Diagnostics Pseudomonas cepacia lipase in propan-1-ol T=20°C; pH=7.0; Enzymatic reaction; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 14, # 24 p. 3917 - 3924
反应条件
Bacillus coagulans NCIMB 9365 dry cells in water; acetone T=25°C; pH=6.5; 24 h;
参考文献
Tetrahedron Asymmetry, , vol. 16, # 4 p. 841 - 845
反应条件
Bacillus coagulans NCIMB 9365 dry cells in water; acetone T=25°C; pH=6.5; 7 h;
参考文献
Tetrahedron Asymmetry, , vol. 16, # 4 p. 841 - 845
反应条件
Bacillus coagulans NCIMB 9365 dry cells in water; acetone T=25°C; pH=6.5; 7 h;
参考文献
Tetrahedron Asymmetry, , vol. 16, # 4 p. 841 - 845
反应条件
4 A molecular sieve; N-ethyl-N,N-diisopropylamine; (S)-1-methyl-2-[(N-benzyl-N-methylamino)methyl]pyrrolidine in dichloromethane; N,N-dimethyl-formamide T=-78°C; 3 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 16, # 6 p. 1157 - 1165
反应条件
recombinant Escherichia coli esterase YbfF W235I mutant in aq. buffer T=30°C; pH=7.5; Enzymatic reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 16 p. 3009 - 3015
反应条件
recombinant Escherichia coli esterase YbfF W235E mutant in aq. buffer T=30°C; pH=7.5; Enzymatic reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 354, # 16 p. 3009 - 3015
反应条件
n-butyric anhydride; sodium hydroxide; lipase AK 1.) H2O, 2.) diisopropyl ether, 0-1 deg C, 8.5 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 23 p. 3459 - 3464
反应条件
1: 85 percent / <PdCl2(PhCN)2> / tetrahydrofuran / 3 h / 20 °C View Scheme
参考文献
Tetrahedron, , vol. 48, # 6 p. 1071 - 1080
反应条件
potassium hydroxide in methanol; water 1.) 0 deg C, 1 h, 2.) room temp., 5 h;
参考文献
Mukaiyama, Teruaki; Tanabe, Yoo; Shimizu, Makoto
Chemistry Letters, 1984 , p. 401 - 404
