双(2,4-二硝基苯)二硫化碳合成路线 (共 81 条)
反应条件
tetramethylstannane; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; 4 h; other reagents: tetraethylstannane, hexamethyldistannane, tributylvinylstannane, tetracyclohexylstannane, tetraphenylstannane, cyclohexene, tetramethylgermane;
参考文献
Cochran, John C.; Friedman, Susan R.; Frazier, John P.
Journal of Organic Chemistry, 1996 , vol. 61, # 4 p. 1533 - 1536
反应条件
CoCl2 in acetonitrile Ambient temperature;
参考文献
Chowdhury, Shantanu; Samuel, Purnima M.; Das, Indira; Roy, Sujit
Journal of the Chemical Society, Chemical Communications, 1994 , # 17 p. 1993 - 1994
反应条件
C3H3NNH in dichloromethane 2 h; Ambient temperature;
参考文献
Sosnovsky, George; Krogh, James A.
Liebigs Annalen der Chemie, 1982 , # 1 p. 121 - 136
反应条件
selenium; sodium thiosulfate in dimethyl sulfoxide
参考文献
Battistoni, Paolo; Bompadre, Stefano; Bruni, Paolo; Fava, Gabriele
Gazzetta Chimica Italiana, 1981 , vol. 111, # 11/12 p. 505 - 508
反应条件
disodium salt of the dianion of 1,4-dinitrocyclooctatetraene in tetrahydrofuran T=-60 - -50°C; 0.15 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 35, # 11 p. 2375 - 2378
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2590 - 2593
反应条件
sodium ethanolate in ethanol T=50°C; 3 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, p. 807 - 808
Zhurnal Organicheskoi Khimii, , vol. 20, # 4 p. 889 - 890
反应条件
tetramethylstannane; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; 4 h; other sulfenyl halides, other reagents: tetraethylstannane, hexamethyldistannane, tributylvinylstannane, tetracyclohexylstannane, tetraphenylstannane, cyclohexene, tetramethylgermane, other solvent: THF-d8; Mechanism;
参考文献
Cochran, John C.; Friedman, Susan R.; Frazier, John P.
Journal of Organic Chemistry, 1996 , vol. 61, # 4 p. 1533 - 1536
反应条件
in ethanol T=50°C; 30 h; Yields of byproduct given;
参考文献
Cardellini, Mario; Cingolani, Gian Mario; Claudi, Francesco; Gulini, Ugo; Martelli, Sante
Synthesis, 1980 , # 11 p. 886 - 887
反应条件
in ethanol T=65°C; 18 h; Yields of byproduct given;
参考文献
Cardellini, Mario; Cingolani, Gian Mario; Claudi, Francesco; Gulini, Ugo; Martelli, Sante
Synthesis, 1980 , # 11 p. 886 - 887
反应条件
sodium ethanolate; cyanoacetic acid ethyl ester in ethanol T=50°C; 3 h;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, p. 1160 - 1167
Zhurnal Organicheskoi Khimii, , vol. 20, # 6 p. 1276 - 1283