1-(2-硝基苄基)吡咯-2-甲醛合成路线 (共 4 条)
反应条件
sodium hydride 1.) DMF, from 20 deg C to 30 deg C, 2.) DMF, RT; Yield given. Multistep reaction;
参考文献
REDX PHARMA LIMITED; CRAIGHEAD, Mark; PALIN, Ronald; MURRAY, Neil; LINDSAY, Derek
Patent: WO2012/63085 A2, 2012 ;
Location in patent: Page/Page column 90 ;
WO 2012/063085 A2
反应条件
in 1H-pyrrole-2-carboxaldehyde; N,N-dimethyl-formamide; mineral oil
参考文献
American Home Products Corporation
Patent: US5521173 A1, 1996 ;
US 5521173 A
反应条件
palladium monocarbide in dichloromethane; ethyl acetate
参考文献
American Cyanamid Company
Patent: US5733905 A1, 1998 ;
Title/Abstract Full Text Show Details
American Cyanamid Company
Patent: US5516774 A1, 1996 ;
Title/Abstract Full Text Show Details
American Cyanamid Company
Patent: US5736540 A1, 1998 ;
反应条件
hydrogen; palladium on activated charcoal in ethanol Ambient temperature;
参考文献
Craighead, Mark; Palin, Ronald; Murray, Neil; Lindsay, Derek
Patent: US2013/225594 A1, 2013 ;
Location in patent: Paragraph 0303 ;