in dichloro difluoro methane 1.) -150 deg C to -30 deg C, 24 h; 2.) -30 deg C to 22 deg C, 0.2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Johri, Kamalesh K.; DesMarteau, Darryl D.
Journal of Organic Chemistry, 1983 , vol. 48, # 2 p. 242 - 250