2-氯-3-甲基-[1,3,2]氧氮杂-磷杂环戊烷合成路线 （共 9 条）
反应条件
phosphorus trichoride in diethyl ether T=-50 - 20°C; 4 h;
参考文献
Artyushin, Oleg; Odinets, Irina; Goryunov, Evgenii; Fedyanin, Ivan; Lyssenko, Konstantin; Mastryukova, Tatyana; Roeschenthaler, Gerd-Volker; Kegl, Tamas; Keglevich, Gyoergy; Kollar, Laszlo
Journal of Organometallic Chemistry, 2006 , vol. 691, # 26 p. 5547 - 5559
反应条件
triethylamine; phosphorus trichoride in dichloromethane a. -30 deg C to RT, b. RT, 2h;
参考文献
McGuigan, Christopher; Swords, Bernadette
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , p. 783 - 787
反应条件
2-chloro-1,3,2-benzodioxaphosphole T=-25°C;
参考文献
Pudovik, M. A.; Ostanina, I. L.; Pudovik, A. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 4 p. 821 - 824
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 4 p. 903 - 907
参考文献
Pudovik, M. A.; Ostanina, I. L.; Pudovik, A. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 4 p. 821 - 824
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 4 p. 903 - 907
参考文献
Pudovik, M. A.; Ostanina, I. L.; Pudovik, A. N.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 4 p. 821 - 824
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 4 p. 903 - 907
反应条件
triethylamine in dichloromethane
T=-60°C; Yield given;
参考文献
McGuigan, Christopher
Journal of the Chemical Society, Chemical Communications, 1986 , # 7 p. 533 - 534
反应条件
triethylamine in diethyl ether
T=-40 - 20°C;
参考文献
Denney, Donald B.; Denney, Dorothy Z.; Liu, Lun-Tsu
Phosphorus and Sulfur and the Related Elements, 1985 , vol. 22, p. 71 - 84
反应条件
triethylamine in benzene
参考文献
Pudovik, M. A.; Kibardina, L. K.; Pudovik, A. N.
J. Gen. Chem. USSR (Engl. Transl.), 1982 , vol. 52, # 7 p. 1481 - 1487,1310 - 1314
参考文献
Pudovik,M.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1977 , vol. 26, # 3 p. 608 - 610
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1977 , vol. 26, # 3 p. 672 - 675
