N,N-二苄基-1-丙胺合成路线 （共 10 条）
反应条件
ammonium cerium(IV) nitrate in acetonitrile T=20°C;
参考文献
Bull, Steven D.; Davies, Stephen G.; Fenton, Carry; Mulvaney, Andrew W.; Shyam Prasad; Smith, Andrew D.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 22 p. 3765 - 3774
反应条件
acetic acid; zinc; copper(l) iodide in water; dimethyl sulfoxide
T=30°C; 2 h;
参考文献
Estevam, Idalia H. S.; Da Silva, Margarete F.; Bieber, Lothar W.
Tetrahedron Letters, 2005 , vol. 46, # 44 p. 7601 - 7604
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in hexane; toluene
T=20°C; P=30400 Torr; 24 h;
参考文献
Shi; Shen
Helvetica Chimica Acta, 2001 , vol. 84, # 11 p. 3357 - 3365
反应条件
1: With trifluoromethylsulfonic anhydride in dichloromethane
T=0 - 5°C; 0.5 h;
2: With sodium tetrahydroborate in tetrahydrofuran; dichloromethane
T=20°C;
参考文献
Xiang, Shao-Hua; Xu, Jian; Yuan, Hong-Qiu; Huang, Pei-Qiang
Synlett, 2010 , # 12 p. 1829 - 1832
反应条件
[(1,3-bis(2,4,6-trimethylphenyl) imidazol-2-ylidene)Fe(CO)4]; 4,4,5,5-tetramethyl-[1,3,2]dioxaborolane in neat (no solvent)
T=20°C; 24 h; Inert atmosphereUV-irradiation;
参考文献
Zheng, Jianxia; Sortais, Jean-Baptiste; Darcel, Christophe
ChemCatChem, 2014 , vol. 6, # 3 p. 763 - 766
反应条件
1: With trimethyl orthoformate in methanol
T=20°C; pH=6;
2: With sodium tetrahydroborate in methanol
T=0°C; 16 h; Further stages.;
参考文献
Bull, Steven D.; Davies, Stephen G.; Fenton, Carry; Mulvaney, Andrew W.; Shyam Prasad; Smith, Andrew D.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 22 p. 3765 - 3774
反应条件
trimethylamine borane in xylene
7 h; Heating;
参考文献
Trapani, Giuseppe; Reho, Antonia; Latrofa, Andrea
Synthesis, 1983 , # 12 p. 1013 - 1014
反应条件
1: N-benzylidene benzylamine With dimethylsulfide borane complex in toluene
T=45°C; 24 h; Inert atmosphere;
2: propionaldehyde in toluene
T=45°C; 24 h; Inert atmosphere;
参考文献
Tokizane, Masashi; Sato, Kaori; Sakami, Yuki; Imori, Yoichiro; Matsuo, Chika; Ohta, Tetsuo; Ito, Yoshihiko
Synthesis, 2010 , # 1 p. 36 - 42
反应条件
1.1: 90 percent / aq. CAN / acetonitrile / 20 °C
2.1: HC(OMe)3 / methanol / 20 °C / pH 6
2.2: 74 percent / NaBH4 / methanol / 16 h / 0 °C
View Scheme
参考文献
Bull, Steven D.; Davies, Stephen G.; Fenton, Carry; Mulvaney, Andrew W.; Shyam Prasad; Smith, Andrew D.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 22 p. 3765 - 3774
参考文献
Shapiro et al.
Journal of the American Chemical Society, 1959 , vol. 81, p. 3725,3726
