1-苯基-1-环己基甲腈合成路线 （共 19 条）
反应条件
sodium hexamethyldisilazane; Verkade nonionic superbase; palladium diacetate in toluene T=90°C; 6 h;
参考文献
Angewandte Chemie - International Edition, , vol. 42, # 41 p. 5051 - 5053
反应条件
tris(dibenzylideneacetone)dipalladium (0); ZnF2; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=90°C; 24 h;
参考文献
Journal of the American Chemical Society, , vol. 127, # 45 p. 15824 - 15832
反应条件
tin(IV) chloride in dichloromethane T=0°C; 0.166667 h;
参考文献
Tetrahedron, , vol. 46, # 18 p. 6331 - 6342
反应条件
1: trimethylsilyl cyanide With trifluorormethanesulfonic acid in 2,3,4-trifluorotoluene T=-20°C; 0.0833333 h; Inert atmosphere; 2: 1-phenylcyclohex-1-ene in 2,3,4-trifluorotoluene T=-20 - 20°C; Inert atmosphere;
参考文献
Organic Letters, , vol. 11, # 22 p. 5286 - 5289
反应条件
bis(η3-allyl-μ-chloropalladium(II)); 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in 1,3,5-trimethyl-benzene T=20 - 140°C; 10.1667 h; Inert atmosphereSealed tube; chemoselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 19 p. 4470 - 4474
反应条件
sodium hydride in diethyl ether; dimethyl sulfoxide
参考文献
Journal of Organic Chemistry, , vol. 36, p. 1308 - 1309
反应条件
formaldehyd; formic acid; acetonitrile 12 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 61, # 19 p. 6486 - 6487
反应条件
ammonia; sodium amide anschliessend mit einer Loesung von 1.5-Dibrom-pentan (1 Mol) in Aether bei -50grad und Erwaermen des mit Aether oder Toluol versetzten Reaktionsgemisches;
参考文献
Journal of the American Chemical Society, , vol. 68, p. 2345,2348
Journal of the American Chemical Society, , vol. 69, p. 2902,2904
参考文献
Journal of the American Chemical Society, , vol. 74, p. 4059,4062
反应条件
1: potassium tert-butylate / ethanol; water / Inert atmosphere; Heating 2: bis(η3-allyl-μ-chloropalladium(II)); 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene / 1,3,5-trimethyl-benzene / 10.17 h / 20 - 140 °C / Inert atmosphere; Sealed tube View Scheme
参考文献
Angewandte Chemie - International Edition, , vol. 50, # 19 p. 4470 - 4474
