5-氰基-2-甲氧基苯甲醛合成路线 （共 7 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) in DMF (N,N-dimethyl-formamide) T=20°C; 3 h;
参考文献
Assens, Jean-Louis; Bernhart, Claude; Cabanel-Haudricourt, Frederique; Nisato, Dino
Patent: US2004/10011 A1, 2004 ;
Location in patent: Page/Page column 26 ;
反应条件
in methanol 2 h; Inert atmosphereReflux;
参考文献
BIOKINESIS; CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE; BOUGERET, Cécile; GUILLOU, Catherine; ROULEAU, Julien; RIVOLLIER, Julie; CARNIATO, Denis
Patent: WO2014/86964 A1, 2014 ;
Location in patent: Page/Page column 47 ;
反应条件
potassium carbonate in N,N-dimethyl-formamide T=60°C; 2 h;
参考文献
Zhang, Guoying; Zhang, Lingli; Hu, Maolin; Cheng, Jiang
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 291 - 294
反应条件
copper(l) iodide; potassium carbonate in N,N-dimethyl-formamide T=60°C; 2 h;
参考文献
Zhang, Guoying; Zhang, Lingli; Hu, Maolin; Cheng, Jiang
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 2-3 p. 291 - 294
反应条件
1: Br2 / acetic acid 2: dimethylformamide / Heating View Scheme
参考文献
Laali, Kenneth K.; Koser, Gerald F.; Subramanyam, Sundar; Forsyth, David A.
Journal of Organic Chemistry, 1993 , vol. 58, # 6 p. 1385 - 1392
反应条件
in N,N-dimethyl-formamide Heating;
参考文献
Laali, Kenneth K.; Koser, Gerald F.; Subramanyam, Sundar; Forsyth, David A.
Journal of Organic Chemistry, 1993 , vol. 58, # 6 p. 1385 - 1392
反应条件
lithium chloride in DMF (N,N-dimethyl-formamide)
参考文献
US2004/10011 A1, ;
Page/Page column 26 ;
