1-(4-碘苯基)丙烷-2-酮合成路线 (共 7 条)
反应条件
tris(trifluoroacetoxy)-λ3-iodane in tetrachloromethane T=23°C; 3 h;
参考文献
Futami; Nishino; Kurosawa
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 10 p. 3182 - 3186
反应条件
copper(l) iodide; K3PO4*3H2O in dimethyl sulfoxide T=90°C; Inert atmosphere;
参考文献
He, Chuan; Guo, Sheng; Huang, Li; Lei, Aiwen
Journal of the American Chemical Society, 2010 , vol. 132, # 24 p. 8273 - 8275
反应条件
1: NH4OAc / acetic acid / 3 h / Heating 2: Fe, FeCl3, aq. HCl / 1 h / Heating View Scheme
参考文献
Binovic,K.; Vrancea,S.
Chimica Therapeutica, 1968 , vol. 3, p. 313 - 320
参考文献
Striegel; Mayer; Wiegrebe; Schlunegger; Siegrist; Aebi
Archiv der Pharmazie, 1992 , vol. 325, # 12 p. 751 - 760
参考文献
Taniguchi, Masashi; Yamamoto, Yoshio; Nishi, Katsuji
Journal of Mass Spectrometry, 2010 , vol. 45, # 12 p. 1473 - 1476
反应条件
formic acid; formamide T=170 - 180°C; 16 h;
参考文献
Binovic,K.; Vrancea,S.
Chimica Therapeutica, 1968 , vol. 3, p. 313 - 320
反应条件
1: (i) NaOiPr, iPrOH, (ii) /BRN= 969135/
2: HCONH2, HCO2H / 16 h / 170 - 180 °C
View Scheme
参考文献
Binovic,K.; Vrancea,S.
Chimica Therapeutica, 1968 , vol. 3, p. 313 - 320