二甲基[二(苯基乙炔基)]硅烷合成路线 (共 15 条)
反应条件
zinc in acetonitrile T=120°C; 5 h; in a sealed tube;
参考文献
Sugita, Hikaru; Hatanaka, Yasuo; Hiyama, Tamejiro
Tetrahedron Letters, 1995 , vol. 36, # 16 p. 2769 - 2772
反应条件
N,N,N',N,-tetramethylethylenediamine in acetonitrile T=100°C; 12 h;
参考文献
Sugita, Hikaru; Hatanaka, Yasuo; Hiyama, Tamejiro
Chemistry Letters, 1996 , # 5 p. 379 - 380
参考文献
Skonieczny, Janusz; Latos-Grazynski, Lechoslaw; Szterenberg, Ludmila
Chemistry - A European Journal, 2008 , vol. 14, # 16 p. 4861 - 4874
反应条件
in tetrahydrofuran T=-78 - 20°C; Inert atmosphere;
参考文献
Dierker, Gereon; Ugolotti, Juri; Kehr, Gerald; Froehlich, Roland; Erker, Gerhard
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 7-8 p. 1080 - 1088
参考文献
Gmelin Handbook: Co: Org.Verb.2, 4.2, page 192 - 200
反应条件
in diethyl ether 6 h; Heating;
参考文献
Koester, Roland; Seidel, Guenter; Suess, Juergen; Wrackmeyer, Bernd
Chemische Berichte, 1993 , vol. 126, # 5 p. 1107 - 1114
参考文献
Komarov, N. V.; Ol'khovskaya, L. I.; Pushkareva, K. S.; Soboleva, L. A.
J. Gen. Chem. USSR (Engl. Transl.), 1984 , vol. 54, # 7 p. 1584 - 1587,1409 - 1411
参考文献
Bogoradovskii, E. T.
J. Gen. Chem. USSR (Engl. Transl.), 1992 , vol. 62, # 4.2. p. 957 - 958,787 - 788
参考文献
Hoffmann, Florian; Wagler, Joerg; Roewer, Gerhard
European Journal of Inorganic Chemistry, 2010 , # 7 p. 1133 - 1142
反应条件
in toluene T=110°C; Condensation; rearrangement; 4 h;
参考文献
Mathey, Francois; Mercier, Francois; Le Floch, Pascal
Phosphorus, Sulfur and Silicon and Related Elements, 1999 , vol. 144-146, p. 251 - 256